GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020513\10132 .D Vial : 19 Acq On : 14 May 2002 6:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Acetonitrile, dichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

3.64 0.46 ug/1 37515 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 2 Allyl/mercaptan 74 C3H6S 000870-23-5 9 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 9 4 N-Nitrosodimethylamine____________ 74 C2H6N2O 000062-75-9 7 Abundance / Scan 96 (3.643 min): 10132.D (-92) (-) m/z 74.00 100.00% / 74 82 5000 47 38 A T I» । i ' । 'r-r-p-r fA-—— 3.20 3.40 3.60 3.80 4.00 ■ ■ i ■ • • ■ । । r i r I11 1 1 I...I, I1 1 59..... 1 88 108 - ■ । ■ ■ ■ ■ । ■ ■ ■ i’i ■ ■ ■ ■ i m/z 81.90 54.34% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 l , A) al , I SA 3.20 3.40 3.60 3.80 4.00 47 m/z 84.00 52.93% 35 12 26 n/z-> | । ■ ■ ■ | । ri'. 10 20 :30 । । 1 |-i ’ । 40 Il50. 6062.70 ' TIB80 , । |

90 108 । | । । I lr-i--i • ।

100 110 Abundance #28161: Allyl mercaptan 41 74 "lIt 1 ■ 1 I 1 ' 1 ' I ■ ■ • l ■ ■ • > l ■ ■ 3.20 3.40 3.60 3.80 4.00 5000 m/z 47.10 37.34%

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/z—> —1 1153.58.5841 10 20 27 33 1 30 40 50 60 70 ‘ ' i ' 1 ' ' i ■ ■ ' ■ i ' 1 ' ' Ti 80 90 100 110 i ) PAMwMMAMhMMoAp Abundance #115342: Acetonitrile, dichloro- 74 3.20 3.40 3.60 3.80 4.00 35 m/z 76.00 32.85%

5000 82

47

— ———————— Pmmmmm TDl 1 ■ i ' ' 1 1 i ■ 1 ■ ■ i ■ ‘ 1 ■ i ............... A AA........... m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

10132.D SCAN020507 .M Wed May 15 09:54:26 2002 Page 4

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