GCMS analysis results for sample AE10812, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\10812.D Vial: 18 Acq On : 22 May 2002 1:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.66 0.29 ug/1 21432 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 2 Allyl mercaptan 74 C3H6S 000870-23-5 9 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 9 4 1-1ropanethiol 76 C3H8S 000107-03-9 7 Abundance Scan 98 (3.655 min): 10812.D (-95) (-) m/ z 74.10 100.00% 74

5000 47 82

38 +14/4 i ' " -A 3.40 3.60 3.80 4.00

n/z-> 01 -llll 58,—711 10 20 30 40 50 60 70 ■ ■ । 1 ■ ■ ■ । ‘ 100 110 ■ । m/ Z 76.00 53.71% Abundance #28338: Acetonitrile, dichloro- 74

5000 82 47 3.40 3.60 3.80 4.00 m/z 81.90 48.14% 35 12 26 | ,|, , 108 m/z-> 01 ' ' I ' 1 ' 1 1 ' 1,1,1 1 1 11 1 I i 1 1 10 20 30 40 111112 50 60 ....70 ' Tilil 80 i, । Tmmin ..... ............. 90 100 110 Abundance #28161: Allyl mercaptan 41 74 4. A-A--Ap 3.40 3.60 3.80 4.00 5000 m/z 47.05 42.40%

n/z-> Abundance Of .......... 10 20 30 40I 47 +153.58—468,41 50 60 70 80 1 1 i ' ■ ■ ■ i ‘

#115342: Acetonitrile, dichloro- 90 ■ i ■ ' ■ ■ i ■ ■ • ■ i 100 110 hus WA"WMAWWAMy 74 3.40 3.60 3.80 4.00 35 m/z 84.00 30.39% 5000 47 82 WhhshwtsiWi 0 ' ^1 1 ' 1.... . I '' TO3 1 ' i ■ ' ' ■ 1 1 1 1 ' 1 1 1 1 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 3.40 3.60 3.80 4.00

10812.D SCAN020521.M Fri May 24 09:21:53 2002 Page 3

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