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GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10131 on May 17, 2002.

NYC-WTC_000046170–000046179

Folder label: “GCMS X 5/7/02 A 5/14/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10131.D Vial: 18 Acq On : 14 May 2002 5:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 37166 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 83 2 Phosphonic acid, (3-methyl-3-pen... 188 C8H13O3P 022152-34-7 50 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 47 4 Pentacyclo[8.4.0.0(3,7) .0(4,14) .... 188 C14H20 1000099-27-2 45 Abundance Scan 4915 (31.958 min): 10131 .D (-4907) (-) m/z 188.15 100.00% 188

5000

> | "' ■ ‘ ' | 1 ■ ' T 'I ' 1 > > | > 1 > > l 1 80 122 . 31 60 31.80 32.00 32.20 49 I 1109 1.158 , r a ■ > 1 1 r1 - 1 1 । 1 1 1 ' 1 1 248 1 1 ■ 421 m/ z 189.20 19.71% m/z-> 50 100 150 200 250 300 350 400 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 94 m/z 80.10 16.30% 160 , 17 4266, 1, , 132.4 J1dl 1 1 ' ' I ' 1 1 1 I' ' 1 i 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #79704: Phosphonic acid, (3-methyl-3-penten-1 -ynyl)-, dime... 188

31.60 31.80 32.00 32.20 5000 77 m/ z 94.10 15.75% 35 , 109 155

m/z-> Alalksk k, 1.12811 I 50 I 1 100 1 ' r I 150 1 1 200 250 300 1 350 i ■ 400 /....................................... Abundance #79806: Naphthalene, 2,6-dimethoxy- 188 31.60 31.80 32.00 32.20 m/ Z 132.10 12.57% 145 5000 102 28 1 63 1 4 AM,.I . . Tl ' ' i ' 1 kl 1 i ' 1kums **i >1111,11,1, /z-> 50 100 150 200 250 300 350 400 31.60 31.80 32.00 32.20

10131.D SCAN020507.M Tue May 14 16:00:21 2002 Page 5

NYC-WTC_000046178

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