GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516 11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integratof) e* Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 19 Undecane Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 20.08 0.60 ug/1 43334 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane 156 C11H24 001120-21-4 53 2 Heptadecane 240 C17H36 000629-78-7 53 3 Nonane, 2-methyl-5-propyl- 184 C13H28 031081-17-1 50 4 Dodecane 170 C12H26 000112-40-3 50 Abundance Scan 2894 (20.083 min): 11284.D (-2880) (-) m/z 57.20 100.00% 57

43 71

5000 85 <||>| A era/ A Anwthaw, 19,80 20.00 20.20 20,40 ‘ i ■ • ■ • i . . Il , I 11 16rrI J 99 112 ■ • 'i ■11 ■ । ‘ । 179 ' i ■ ■ • ■ । • • ■ ■ । ■ ■ • ■ ।11 ■ ■ । ■1 m/z 71.20 68.43% niz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #109663: Undecane 43 57

5000 8 ,A Ah, A,AA 71 19.80 20.00 20.20 20.40 29 85 m/z43.1565.73% —TTnr 4 14 99 113 127 .156 ............ miz-> 20 40i 60 80 100 120 140 160 180 200 220 240 Abundance #112319: Heptadecane 57 43 wa"rrW/HA, Mrewt* 71 19.80 20,00 20,20 20.40 5000 m/z 41.10 42.24% 85 29

—— „ 99 113 127 141 1 . । T. . . । .. 1‘ 155 169 183 f। । । 240 । . I 1 । । । l 1 । । । i niz-> Abundance 20 40 60 57 80 100 120 140 160 180 #17101: Nonane, 2-methyl-5-propyl- 200 220 240 wMMhAWAanh 19.80 20.00 20.20 20.40 43 71 m/z 85.00 31.71% 5000 85 29

m/z—> -1" 20 40 I l' |I 99 112 126 140 155 " t 1 , 1a a .1 ,a h, 60 80 100 120 140 160 180 200 220 240 , ‘ ' I ' AM, 19.80 20.00 20.20 20.40

11284.D SCAN020507.M Fri May 17 13:06:52 2002 Page 22

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