GCMS analysis page for sample AE11569, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11569.D Vial: 22 Acq On : 22 May 2002 5:06 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 3-Heptenoic acid, 5-hydroxy... Concentration Rank 2 R.T. EstConc Area Relative to. ISTD R.T. 42.53 0.43 ug/1 25059 Perylene-dl2 43.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Heptenoic acid, 5-hydroxy-2,6,... 186 C10H18O3 110678-37-0 16 2 Undecane, 6-ethyl- 184 C13H28 017312-60-6 12 3 dl-2-Ethylhexyl chloroformate 192 C9H17C1O2 024468-13-1 12 4 1-Decanol, 2-methyl- 172 C11H240 018675-24-6 10 Abundane Scan 6714 (42.528 min): 11569.D (-6703) (-) m/ z 57.20 100.00% 57

5000 185 41 70 112 83 98 207 AA.AA4 ial HWHi ul d 125 224 42.20 42.40 42.60 42.80 n/z-> O—P 20 60 "f 80 Cai 100 I. 120 140 160 -. 1, 151 I ■ । ■ ■ ■ 1 i 1 1 ■ 1 i 1 1 1 1 i 1 180 200 220 m/z 185.10 45.22% Abundance #17579: 3-Heptenoic acid, 5-hydroxy-2,6,6-trimethyl-, [r*,... 57

112 5000

ux 4— 41 42.20 42.40 42.60 42.80 83 29 130 m/z 112.10 37.19% 0+4— I 141 153 168 186 ■' 111 *11*111* *11*111* n/z—> 20। 40 60 80 100 120 140 160 180 200 220 Abundance #112361: Undecane, 6-ethyl- 57 1 ' i ■ ■ i ■ ■ ■ ■ i 43 71 42.20 42.40 42.60 42.80 5000 m/z 70.20 36.45% 29 85 119 0- ' ' । ,1 H , p14— 125. 140 154 , 184 , ... miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #17577: dl-2-Ethylhexyl chloroformate 1’’ ..I’" 57 70 112 42.20 42.40 42.60 42.80 m/z 55.10 34.80% 5000 83 43

n/z-> O-I 20 60 ————— 80 I

100 97 129 149 120 140 160 180 192 200 220 ukhdadi 42.20 42.40 42.60 42.80

11569.D SCAN020521.M Fri May 24 09:44:10 2002 Page 6

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