GCMS surrogate recovery results, sample AE07110, April 15, 2002

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. Data File : C:\MSDCHEM\l\DATA\041002\7110.D vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L

Peak Number 20 Tetratriacontane $$ n-Tetra... Concentration Rank 15

R.T. EstCoiic Area Relative to ISTD R.T. i

36.68 2.27 |ug/L .208179 Perylene-dl2 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 80 2 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 80 3 Octacosane 394 C28H58 000630-02-4 74 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 74 Abundance Scan 5719 (36.682 min): 7110.D (-) m/z 57.10 100.00% 57

aSB 85

113 141 36.40 36.60 36.80 37.00 208 0- I I I m/z 71.15 60.44% Ti/Z~> 0 50 100 150 200 250 300 350 400 Abundance #363627; Tetratriacontane $S n-Tetratriacontane (7

5000 85 36.40 36.60 36.80 37.00 m/z 85.15 36.27% 29 0- it . J j jyj^,iy.225 2^ 281 311337 367 ^10435

m/z-> 0 50 100 150 200 250 300 350 400 Abundance I #329266: Octacosane $S n-Octacosane 57

36.40 36.60 36.80 37.00 5000 m/z 43720 37796% 85

29 ‘113 0- n/z-> 0 50 100 150 200 250 300 350 400 Abundance #329268: Octacosane 7 36.40 36.60 36.80 37.00 m/z 55.10 31.76%

MW 85

113 183211 239 267 309 337 394 0- ■n/z~> 0 50 100 150 200 250 300 350 400 36.40 36.60 36.80 37.00

7110.D 5080402BB.M Mon Apr 15 17:09:31 2002 Page 22

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