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GCMS analysis results for sample AE00466, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Cyclohexane, octyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 23.56 0.40 ug/L 238230 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, octyl- 196 C14H28 001795-15-9 53 >1(9 2 Cyclohexane, 1,1‘-(1,4-butanediy... 222 C16H30 006165-44-2 52 3 Hexane, 1,6-dicyclohexyl- $$ Cyc... 250 C18H34 001610-23-7 50 4 Cyclohexane, hexyl- 168 C12H24 004292-75-5 49 MAT Abundance Scan 1768 (23.559 min): 00473.D (-) m/z 83.10 100.00% 55 83 /WAPA/ wwVU 5000 97 67 41 li I 111123 137 153165 186199 221 235 249 264 278 23.20 23.40 23.60 23.80 O-TT ., il.i , ■ ‘ । ■' " "h r hh,1 l""tz 1 hept 1h h 1 1.h,, lah hphi"_ 1.,. m/z 55.10 89.45% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #110350: Cyclohexane, octyl- 55 83

5000 23.'20 23.40 23.'60 23.80 ' 67 m/z 82.10 87.71% 27 42 । । 01.1.1. ’ ' 1 i 1 ' 1 1 । ' 1 1 1 । 1 1 • 11 • • • 1 । 1 1 11 । 1 * 1 1 । 1 1 1 । । 1 1 1 1 । 1 1 1 • । 1 ■ 1 97 112 196 n/z-> Abundance r I * • ■ ' I 1 ‘ ' 1 1 ......... 1 1 :20 40 60 80) 100 120 140 160 180 200 220 240 260 280 AA/UAm #148920: Cyclohexane, 1,1 '-(1,4-butanediyl)bis- (CAS) $$ 1... 83 55 ' 1 ■ ■ ■ 1 1 ■ ■ ■ 1 1 ■ 1 ■ ■ । ■ 1 1 1 1 ■ 23.20 23.40 23.60 23.80 5000 m/z 97.10 49.31% 67 139 96 ] 222 n/z-> 0 i 1 1 1 1 1 1 r 20 40 Ji J 60 .. C?9.,.. 80 100 120 140 160 180 200 220 240 260 280 Abundance #187773: Hexane, 1,6-dicyclohexyl- $$ Cyclohexane, 1,1'-(1... 83 23.20 23.40 23.60 23.80 m/z 95.10 37.90% 55 5000

67 96 0-PTTT Ji i .li1. ■ A+199TTTTTTTTETTT"166 222 ‘TIT‘‘EII"1IITT 250 L ‘I*I‘I‘IT‘U 11 !' 111 I 1 m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 23.20 23.40 23.60 23.80

)0473.D SCAN508.M Fri Jan 11 10:09:09 2002 Page 8

NYC-WTC_000051274

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