GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.43 ug/L 530721 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-D10 188 C14D10 000000-00-0 91 3 Anthracene-diO- 188 C14D10 001719-06-8 78 4 Acridine-D9 188 C13D9N 000000-00-0 50 Abundance Scan 1699 (22.771 min): 00028A.D (-) m/z 188.15 100.00% 188

5000

m/z-> Abundance 42 52 0- TWTPITTTT 66 — 80 108 136 146 ■ I ■ ■ । f l ■1 * ■ I ■ ■ । ■ 11'1' 1'1 f' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 T’Trnl

#84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 s.. 22.40 22.60 22.80 23.00 23.20 m/z 189.20 18.12%

188

5000 ......................... ............. 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 94.10 16.08% 158

Tl/Z-> 0- ■<।•■ •■ । 66 mIt 11111111'11111 ri ■ i • • l ■ । • । ।।। < 111‘| ।1 ■ ■ । ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 slamn Abundance #84498: Anthracene-D10 188 -- 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.09% 80 94

nfz-> . 0- '' i'1 " i' 66 ' 1111111 " 1 • । > 1111' 111 > । 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 ll 111 ............ .... .................................... Abundance #84502: Anthracene-d1 0- 188 22.40 22.60 22.80 23.00 23.20 m/ z 80.10 10.64%

5000

80 94

m/z-> 0 66 —mPPPIPP 40 50 60 70 80 160 ....... ................ " 111'' I'''11' " ' 111'111 ‘‘ 11 90 100 110 120 130 140 150 160 170 180 190 ......1........... 22.40 22.60 22.80 23.00 23.20

00028A.D HP020702.M Thu Feb 21 15:48:54 2002 Page 14

NYC-WTC_000004857

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