GCMS analysis results for sample AE03246, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On : 1 Mar 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.46 ug/L 360110 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 80 2 Anthracene -p 10 188 C14D10 000000-00-0 80 3Anthracene/dl0 - 4 Phenanthrene - dl 0 Abundance 188 C14D10 188 C14D10 KM7 Scan 1718 (22.768 min): 03246.D (-) 001719-06-8 78 001517-22-2 64 m/z 188.10 100.00% its

5000

80 94 42 52 66 132 146 160 22.40 22.60 22.80 23.00 Of Ttt 11111 ■11111" i'"1111111111 |’’ 111 111 ‘‘ I’T m/z 189.10 21.25% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 -------------------------------- 22.40 22.60 22.80 23.00 80 94 m/ z 94.00 20.21% 66 I ■ ■ • • 111 ■ ■ । ■ - ■ ■ । ................ .. 158 | I । TTII I | I I I l'| I I I , | I I ! I 111'l1!1! < > 11 01 - ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ I. ।. TIT

n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188 ------- 22.40 22.60 22.80 23.00 5000 m/z 80.00 17.63% 80 94 66 160 —— Ol " I " " I " 111 " ।111 " m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d ID- 188 22.40 22.60 22.80 23.00 m/z 184.05 15.38%

5000

80 94 160 , , 66 - m/z-> 0 TIPTTTTT — 44+1Ql—— 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22,40 22.60 22.80 23.00

)3246.D HP022102.M Mon Mar 04 12:33:14 2002 Page 14

NYC-WTC_000006122