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← Document results/DEP Box 28/GCMS X 1/11/02 A 1/31/02
Document / 19 pages

GCMS analysis results for sample AE00833, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.

NYC-WTC_000052069–000052087

Folder label: “GCMS X 1/11/02 A 1/31/02”

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Scanned page image, NYC-WTC_000052083
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : January 31, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 4-HYDROXY-BICYCLO[2.2.2]OCT... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

16.55 0.05 ug/L 39807 Ac enapht hene-d10 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-HYDROXY-BICYCLO[2.2.2]OCTANONE... 140 C8H12O2 066348-59-2 49 2 .beta.,beta.-Difluorostyrene 140 C8H6F2 000000-00-0 9 3 4H-Pyran-4-one, 2-ethyl-3-hydroxy- 140 C7H803 004940-11-8 9 4 3-Pyridinecarboxylic acid, 1,2,5... 155 C8H13N02 000063-75-2 9 Abundance Scan 1154 (16.549 min): 00833.D (-) m/z 140,10 100.00% 140

5000 122 172 .r r i r , (■ , i , , । i 43 56 71 89 16.20 16.40 16.60 16.80 — o1 ' 1 I' I,.1 ' 1 I I „' ' ■ i1 ■ ■ ■ i‘ 11 11' ■ • i' ■ TTT m/z 172.20 30.26% n/z—> 40 50 60 90 100 110 120 130 140 150 160 170 70 80 Abundance #35653: 4-HYDROXY-BICYCLO[2.2.2]OCTANONE $$ Bicyclo[2.2.2]... 83 140 55 70 97 112 5000 , . .............. 1620 16.40 16.60 16.80 m/z 122.20 27.14% 125 0- 1 ■ i ■ ■ ■11 11 TTur I’’ 11'1 "n ........I i ■ •1 • I n I ' r ■ ■ i i1 ‘ ‘111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35448: .beta.,beta.-Difluorostyrene 140 ........ II.......... 90 16.20 16.40 16.60 16.80 ' 5000 m/z 56.10 23.19%

114

mlz-> 0 r > > i ■ I ■ • ■ 11 >■i ■ 11111•I 40 50 60 vrp - 101 L 1............................... 70 80 90 100 110 120 130 140 150 160 170 ■ ’ ■11 1 ' ‘ ■ r ■ 1 ' i 1 ' ■ ' n

Abundance #35344: 4H-Pyran-4-one, 2-ethyl-3-hydroxy- ■p-r TT 140 16.20 16.40 16.60 16.80 m/z 138.10 22.14%

5000 71 55 97 125 /z-> 0 -+40 50 84 I 111 ' i" । ................. TTTTTTTTTTTT I ■ ■ ' ' i 60 70 80 90 100 110 120 130 140 150 160 170 । ■ *111' 16.20 16.40 16.60 16.80

00833 .D SCAN508.M Fri Feb 01 09:18:59 2002 Page 11

NYC-WTC_000052083

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NYC-WTC_000052083Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

machine-extracted · confidence unavailable · Check page ↗

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