DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31219.D Vial: 5 Acq On : 1 Feb 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 . MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************* * * Peak Number 2 3-Pyrrolidinol $$ 3-Hydroxy... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.92 0.04 ug/L 17654 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol $$ 3 -Hydroxypyrro . . . 87 C4H9NO 040499-83-0 5 2 2-Butanone, oxime $$ Butanone ox... 87 C4H9NO 000096-29-7 4 3 2-Butanone, oxime 87 C4H9NO 000096-29-7 4 4 2-Butanone, oxime (CAS) $$ Butan... 87 C4H9NO 000096-29-7 4 Abundance Scan 48 (3.922 min): 31219. D (-) m/ z 75.10 100.00% 75

5000 87 47 55 51 84 3.60 3.80 4.00 4.20 Or ’ I’’’’t+’+11A**AI’E*/#14IIt*AIIT’’’1A ' ‘ I'1" !'11' I' ‘ - ■' 111 “ I' ‘ m/z 87.10 43.95% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4371: 3-Pyrrolidinol $$ 3-Hydroxypyrrolidine 43

. ,, . ................ . 5000 3.60 3.80 4.00 4.20 57 68 87 m/z 55.00 40.30%

miz- > 0- 1l111111—311110111701—1-"7"-""T 128 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 . 541.. Il 'I........... ' i " * * i" 90 95 Abundance #4361: 2-Butanone, oxime $$ Butanone oxime $$ Ethyl methyl... 42 87 , JI..... II f........ 27 3.60 3.80 4.00 4.20 5000 m/z 47.00 32.81% 58 15 31 54 68 72 ob’ ’’1’444 11111111' i • 1111" ’ 1 > 146 TTPT TIITT I 1 1111 ■ *1' 1 " i1 * “ i'1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4360:2-Butanone, oxime 42 3.60 3.80 4.00 4.20 m/z 51.00 24.51% 87 5000 27

54 58 WWWA 46 | 0b " i11 •' i " " I' TIIPp TTTT Hpmp 1 1 i 1 1 1 1 i 1 1 ' ' । ■ 1 1 i ■ ' ■ ' । miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

31219.D SCAN508.M Mon Feb 04 08:41:48 2002 - Page 4

NYC-WTC_000004038

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NYC-WTC_000004038Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999