GCMS analysis report for sample AE01511, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB21\01511.D Vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3.ALPHA.-D1-ANDROST-5-EN-3... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 18.72 0.02 ug/L 15634 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3.ALPHA.-D1-ANDROST-5-EN-3 .BETA.-OL 275 C19H29DO 000000-00-0 74 2 2-Carboxaldehyde-4-vinyl-l, 2,4-t... 163 C10H13NO 000000-00-0 9 3 1-(2-Cyanoethyl)-2-ethyl-4-methy. .. 163 C9H13N3 023996-25-0 9 4 Benzenamine, 2,3,4,5,6-pentameth... 163 C11H17N 002243-30-3 9 Abundance Scan1359(18.715min):01511.D(-) m/ z 80.00 100.00% 80 163

5000

49 * •! • ■ ■ ■ । T T T 18.40 18.60 18.80 19.00 0 i " ■' i ■ ■ ■11 ■ ■' ‘ I • ■ ■ ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ • ‘ ■ i ■ ■ ■ • i • ■ ‘ ■ i' ‘ ■ i ■ • ■11 ■1 rn/z 83.90 89.43% m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #218995: 3.ALPHA.-D1-ANDROST-5-EN-3.BETA.-OL 1(3

5000 A wac . 18.40 18.60 18.80 19.00 m/z 163.10 75.68% 0 10CG* ‘I "Iu /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #63439:2-Carboxaldehyde-4-vinyl-1,2,4-trimethylpyrrole $$... 1(3

18.40 18.60 18.80 19.00 5000 134 m/z 162.10 26.28% 42 56 148

0- a | TT-p-r < i • • • > ।1«> * j *i* ■• • i ‘ • i • • > ‘ i • • ■ • i • ■n-j-rr i ■ ‘1 ‘ i iz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #63307:1-(2-Cyanoethyl)-2-ethyI-4-methylimidazole $$ 1H-I ... L. TII T T TI 1(3 18.40 18.60 18.80 19.00 109 148 m/ z 48.90 17.52%

5000 95 123 W MwW P

54 68 J____ 135 1 0 । > * > > । < । * 11 < ■ * I ‘ ‘ I * ' ‘ * P ’ ’ ’ I ’ *4 1 I 11 ‘ ‘‘‘11‘ ‘11 ‘ ‘ T-TT i ■ ■ ■11 1 ‘ I ’' ‘ 1 I ' ’ ' I * ‘ ‘ I ‘ ’ niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 18,40 18,60 18.80 19.00

31511.D HP022102.M Mon Feb 25 10:55:17 2002 Page 10

NYC-WTC_000010060