DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document LIDrary searcr compound Keport

Data File : C : \MSDCHEM\1\5973N\02FEB27\02387.D Vial: 3 • Acq On : 27 Feb 2002 4:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5 R.T. EstConc • Area Relative to ISTD R.T. 22.28 0.11 ug/L 79445 Phenanthrene-dl0 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 59 3 Phenanthrene, l-methyl- 192 C15H12 000832-69-9 59 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 Abundance Scan 1675 (22.282 min): 02387. D (-) m/z 192.00 100.00% 192

5000

/ 82 96 146 LiB, 70 | 160 22.00 22.20 22.40 22.60 44 i 118 0- 1 ‘ I'1 ’11 1 ‘ ‘111 1 ■ । 11 ■ i > ■ ■ ■ 11 ■ ■ 11,,,. j.,., ।. - — m/z 146.10 17.34% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 A22.00 22.20 22.40 22.60 96 164 m/z 96.00 15.80% 138 01 1 , । . . . , । , . . . , . , , , । . . . , [ , , , . । ,- TamTTTTT T1]n mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103930: Phenanthrene, 2-methyl- 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 14.09%

96 88 J 139 152 165 176 0 '' i ‘ ' i " " i'11' i1 " ' i " '11'11' i ■ " ' i " " i11 ■' i1'111 " ' ‘ i11'11 ‘ 1’1 — TPTTT mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103924: Phenanthrene, 1-methyl- 192 22.00 22.20 22.40 22.60 m/z 82.00 13.40%

5000

m/z—> 0 ...................... I.................... . 1 1 1 * 1 1 1 1 1 1 1 1 1 1 1 * 1 I ‘ ' 1 • I 1 1 1 ' 1 1 1 f 1 I > l ■ I I I ■ 1 I I I < I > [ 1 I 1 l I > ' ■ 1 I I 1 > > [ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 165 178 44 yualjun । U — 22.00 22.20 22.40 22.60

32387.D HP022102.M Thu Feb 28 08:47:17 2002 Page 14

NYC-WTC_000005063

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999