GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB21\0123B.D Vial: 1 Acq On : 21 Feb 2002 10:46 am Operator: Sample : lab blank 1/23 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 2-(Dichloromethyl)tetrahydr. .. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

19.98 0.04 ug/L 27764 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-(Dichloromethyl)tetrahydrofuran 154 C5H8C12O 000000-00-0 9 2 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIM... 186 C8H14N2O3 072700-98-2 5 3 Imidazole-2,4,5-d3 $$ lH-Imidazo. .. 71 C3HD3N2 006745-43-3 4 4 2-Propenamide (CAS) $$ Acrylamid. . . 71 C3H5NO 000079-06-1 3 Abundance Scan 1471 (19.980 min): 0123B.D (-) m/ z 71.10 100.00% 71

43 5000 186 ' i ■ ■ ■ ■ i ■ ' i' ' ■ i ■ ■ ■ ■ i 1 19.60 19.80 20.00 20.20 20.40 0 I “ ‘ * I' • " 1 *1 “ I “4111 r' 11' ‘ " I ’1 “ I ‘" I ‘ ‘' I ........................... 1 TB1000192’11311’8010"TB1T"’1U" ■ i ■" m/z 43.00 49.52% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #51400:2-(Dichloromethyl)tetrahydrofuran 71

5000 43 ■ i ■ ■ • ‘ I ’ 1 ‘ ' 1 ‘ 19.60 19.80 20.00 20.20 20.40 82 m/z 186.00 30.11% 53

Olyunniyuni 1............................................. 1 ‘ • I ‘ ' 11'1 ‘! *' • ‘ 11' ‘11 ‘1 *1!' ‘' 111 ‘ * I'1 ‘ 174 * I I I I »I I * « miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #94657:2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1 -PYRROLINE ... 71 ■ i 1 ■ ■ ' i ' ■ ■ ■ i ■ ' ■ ■ i ' 19.60 19.80 20.00 20.20 20.40 5000 55 116 m/z . 49.00 17.36% 41 186 86 142

0- " I ' ‘‘ I ‘ ‘ “ I " “ 11 " r ‘ “ i" ‘ ' I " Tprrrp-rrrrrT- ‘ I' ‘ ‘ ‘ 1 ‘“ I " ‘ I " " I " " I " 1 ‘ I “ 11''1 AM NV NN miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #1085: Imidazole-2,4,5-d3 $$ 1 H-lmidazole-2,4,5-d3 (CAS) $... ■ i ■ f ' ' i ' 71 19.60 19.80 20.00 20.20 20.40 m/ z 41.10 15.57%

5000 43

16 30 , I 0 " i1 --H i1 r rpmipunt ■ ■ i ■ ■ ■ ■ i ■ ■1 ■ i ■ ■ ■ ■ i1''11 ■1 ■ ■ i ■ ■1 ■ i ■ ■ ■' i"' ■ i ■1 ■ ■ i"' ■ i ■ ■ ■ ■ i ■" miz—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40

0123B.D HP022102.M Mon Feb 25 10:54:38 2002 Page 13

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