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GCMS blank results for VOCs, sample AE12326, June 2002

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Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12326 on June 3, 2002.

NYC-WTC_000014351–000014374

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\LBA.D Vial: 14 Acq On : 29 May 2002 8:41 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Anthracene-dlO- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.28 ug/L 246223 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 58 2 Phenanthrene-diO 188 C14D10 001517-22-2 47 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128.-67-1 42 4 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 42 Abundance Scan 3401 (23.062 min): LBA.D (-3395) (-) m/z 188.10 100.00% US

5000 - 80 94 42 52 66 160 22.80 23.00 23.20 23.40 01009m—m]0—THMH * * i • ■ •' i * ■ • * i * ■" t >' * ‘ i1 ■ HH m/z 80.10 17.05% niz-> Abundance 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 #79826: Anthracene-d10- 188 fl 5000 22.80 23.00 23.20 23.40 m/z 184.10 15.85% 80 94 160 17 30 42 52 66 , 0 TImTTTTTTTTTH +108 118.132.146+1791794—. miz-> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 — T 22.80 23.00 23.20 23.40 5000 m/z 94.20 12.95%

30 42 52 65 160 80 94। 108 118 132 146 II 170179], 0- amammumamman—n— mTTnr VTTT

tJz-> 10 2030405060 70 8090 100110120 130140150160170180190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 11B 22.80 23.00 23.20 23.40 m/z 189.15 11.66% 121 5000 173 67 94 39 57 | 84 0- ' I ‘ ‘' I'' ‘ *[1 111 "u '11'1 ''111 n'l 11111111 11111 > i! 111 133 146 161 Iu , | TTTTIOt* i • ■ ■ m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

LBA.D 052202.M Mon Jun 03 11:28:17 2002 Page 18

NYC-WTC_000014372

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NYC-WTC_000014372Source: NYC Law Department, mirrored locally

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