GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08257.D Vial 15 Acq On : 17 Apr 2002 9:01 pm Operator Nefliu Sample : sample Inst Instrumen Mise : Multiplr 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 10 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

23.17 0.57 ug/L 871894 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Anthracene-dlO - 188 C14D10 001719-06-8 94 2 Phenanthrene-dlO 188 C14D10 001517-22-2 64 3 2,2,9,9-Tetramethyldec-5-ene-3 ,7... 188 C14H20 102745-35-7 52 4 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 50 Abundance Scan 3420 (23 174 min): 08257 D (-3414) (-) m/z 188.10 100.00% 11 8

5000

— 80 94 22 80 2300 23 20 23 40 23 60 42 52 66 । | 108 132 146 160 0 mmmmd TMITTmpt m/z 189.10 14.58% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 A Abundance #79826 Anthracene-d10- 188

...... ...... 5000 22 80 23.00 23.20 23 40 23.60 m/z 184.10 13.80% 80 94 160 | 17 30 4 2 52 00 | I 102 118 132 146 ,i| 170 180|J| 0- | I । > । | I u H I H I | I 1 । I | । I I I | 1 । I I { । । I I | । I I । | I I I । | I I I । | I I । । | I I T I | I । । । | I । I । | I I ‘‘‘ I FT| I I I I f Hrr I I II fl n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ----- 22 80 23.00 23.20 2340 23.60 5000 m/ Z 94.00 12.15%

80 94 160 30 42 52 66 , 1 102110118 132 '146,1 170 181 Ob j ।. ।! । > > IIWTTHTTTTHp TI "n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79801: 2.2.9.9-Tetramethyldec-5-ene-3,7-diyne 188 22 80 2300 23.20 23.40 23.60 173 m/ z 80.10 10.41% 41 131 143 91 5000 77 158 57 119 27 67 105

0-7 Ijuvri L4q II +1 +1+ +444 lITpenur rm /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23 20 23.40 23 60

08257.D 041702SCAN.M Thu Apr 18 09:33:57 2002 Page 15

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