GCMS results sample AE08257, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08257.D Vial: 15 Acq On 17 Apr 2002 9:01 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

12.46 0.31 ug/L 430424 Napthalene-d8 13.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 38 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 28 Abundance Scan 1596 (12.457 mm) 08257.D (-1588) (-) m/z 73.10 100.00% 73 A

5000 267 355 ------------ 40 12.20 12.40 12.60 12.80 oV 125 1WTTUIITTTPPIT 11" "323 177 193 251 L L T" " ।" ■ 'i" m/z 267.00 41.37% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273 Cyclopentasiloxane, decamethy 73

5000 267 . ..... n 12.20 12 40 12 60 12 80 z 355 m/z 355.10 30.25%

n/z--> 20 45 1 96 115 133149165 . 193208223 251 282 307 323339 . 0- 17,‘1011111)"1l 28 40 | -i । "—Hi 11 1** [ 11 T—rrtrrri" 11 v ।! It । । ri IPmaT I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 Id." 355 12 20 12 40 12 60 12 80 267 5000 m/z 3 56.00 10.72%

l| 1111 " 11111323339 1 45 । 191207 223 231 ov —mPmummPTTTPTRTTT ‘r ntnnihum ................................................................................................................................. n/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115268 Benzoic acid, 2-[(trimethylsilyl)oxy}. trimethyl. . . .................... TdiT 73 12 20 12.40 12 60 12 80 m/z 267.90 10.24% 1 5000 267

45 91 151 175 193 209 233 249 11 E 115 135 A 28 ||

0-mTTTUTT L i maum i 'r'|-i l rv| J Aj i I.....|“ Hr | |4| i j I i | i | > t I r I I i I I | | I I I I I i /z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12 20 12.40 12.60 12.80

08257.D 041702SCAN.M Thu Apr 18 09:33:57 2002 Page 13

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