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GCMS blank results for volatile organics, April-May 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.

NYC-WTC_000048085–000048093

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\0409LB.D Vial: 3 Acq On : 19 Apr 2002 10:04 am Operator: Nefliu Sample : 04/09 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Anthracene, 2-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.27 ug/1 539648 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 3 Bitoscanate 192 C8H4N2S2 004044-65-9 52 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 Abundance Scan 4768 (31.094 min): 0409LB.D (-4758) (-) m/z 192.10 100.00% 192

5000 40 146 TTI—T-T———P—TTTT — 82 96 160 30.80 31.00 31.20 31.40

m/z-> 50 70 I , TTTTTWTTWTTTTTTTT H TWTTPTTTPTTTTTTt H 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 m/ z 40.10 31.02% Abundance #125845: Anthracene, 2-methyl- 192

5000 30.80 31.00 31.20 31.40 m/z 191.10 24.41% 75 86 9 115126 139 152 165 176 11".. ।।. 11।. 11"., ।.,., ।, n 11 r. iT| । i'l i-| 1111 |iti 11111111111'| 1111 |'i 1111 iii 111 iti 111 i'i1 ‘IT TTTT n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 192

30.80 31.00 31.20 31.40 64 5000 m/Z 146.10 17.76%

75 90 134 39 50 4 TTTT 18.78+4+4 ,122, , Wt J 107ttp I mlsyh. mm* —h 148 160 — m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125828: Bitoscanate 192 30.80 31.00 31.20 31.40 m/z 193.00 13.64% 5000

134 160 50 63 75 90 102 122

m/z-> " i" " i " " i 176 1111 ■ I Hr" । rlep|l । lh |-t‘i rtehrrh-11 I nil Hrri । J 11111111111 0 10 20 30 40 50 60 70 80 90 100110120130140150160170 180190 200 । 148 I— 30.80 31.00 31.20 31.40

0409LB.D SCAN020418.M Thu May 02 15:22:35 2002 Page 4

NYC-WTC_000048091

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