NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\020415\07979.D Vial: 19
Acq On : 16 Apr 2002 1:32 am Operator: Nefliu
Sample : sample Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 9 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
22.64 0.21 ug/L 256897 Phenanthranene-dl0 23.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 42
2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42
3 3-(2-Methoxy-5-methylphenyl)acry. . . 192 C11H1203 103986-76-1 40
4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 40
Abundance Scan 3330 (22 645 min): 07979 D (-3320) (-) m/z 192.30 100.00%
IS 2
5000
82 96 146 160 22.40 22.60 22.80 23 00
40 4g 70 120
0 --mmPP 4 n. । jJ....... r ... ml . m/z 191.30 20.27%
n/z—>
Abundance
30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
#31030 4-Hydroxy-3,5-dimethylcinnamic acid
192
I
5000
22 40 22 60 22 80 23.00
89 175 m/z 146.30 14.44%
63
45 55 J 77 117 145
| +27/195, Irguu rr I
, 135 h 163
n/z->
0-
30
....40ploli, TITtTpr TT
50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #80953' 2-Propenal, 3-(3,4-dimethoxyphenyl)-
192
161 ................... ....
2240 22 60 22.80 23.00
5000- m/z 193.30 13.33%
77 121 149 177
91 103
138
0- . .... Li....l,i.................. +1
/Z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid
161 192 22 40 22 60 22.80 23.00
m/z 160.30 12.35%
5000 105
77 132
91 115 145
39 51 65
/z—>
0 -lpll
30
—
40 50 60 70 80 90
421l —PPP L
—l+ 1122 .
100 110 120 130 140 150 160 170 180 190 200
175
* 1 i |T.......23.00
22 40 22.60 22 80
1
07979.D 041202SCAN.M Tue Apr 16 13:48:32 2002 Page 12
NYC-WTC_000046737
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