GCMS analysis results for sample AE07632, April 9, 2002

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Laboratory report documenting GCMS analysis of sample AE07632 conducted on April 9, 2002.

NYC-WTC_000047624–000047638

Folder label: “GCMS X 4/4/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07632.D Vial 11 Acq On : 15 Apr 2002 6:58 pm Operator Nefliu Sample : sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.32 ug/L 378239 Phenanthranene-dlO 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 38 4 Naphthalene, 1,7-dimethoxy-__________ 188 C12H1202 005309-18-2 38 Abundance Scan 3420 (23 174 min): 07632 D (-3415) (-) m/z 188.40 100.00% 188

5000

94 160 22 80 23 00 23 20 23.40 23.60 42 52 66 80 132

/z-> 0- TTTTTT n 111111 r " 1 r ■" / ■'1111'11" u'i'1 •' i1 ■ •111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.25 19.27% Abundance #79826 Anthracene-d10- 108

5000- 22.80 23.00 23.20 23.40 23.60 m/z 189.30 15.29% 80 94 160 i 66 0 TWPTNH 17 30 42 52 . 102 118 132 146 ,|| 170 180 TTNTDHt r Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 168 / • I ' TT 22.80 23.00 23.20 2340 23.60 5000 m/z 184.30 12.69%

80 94 160 30 42 52 66 , 102110118 132 146 1 170 180 0-‘■(""I"........... 11' ■ '1111 'I''11'I ■ ■ l'l|' j 111111111 prr ■ 1 11 » I I I I I I I I I . ............ I ■ ■ 111 l1lllllll 11111 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696 2-Quinolinecarboxaldehyde. 8-hydroxy- oxime 168 22 80 23 00 23.20 23.40 23.60 m/z 160.30 11.58% 5000-

143 115

u 89 51 64 76 1 102 I, 130 I 158 170 Tl/Z-> 0 —PTT 10 20 30 40 50 60 70 80 -HH 90 100 110 120 130 140 150 160 170 180 190 22 80 23.00 23.20 23.40 23 60

07632.D 041202SCAN.M Tue Apr 16 13:41:38 2002 Page 10

NYC-WTC_000047637

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NYC-WTC_000047637Source: NYC Law Department, mirrored locally

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