GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.
NYC-WTC_000047886–000047903Folder label: “GCMS X 4/8/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\020417\08256.D Vial 14 . Acq On 17 Apr 2002 8:12 pm Operator Nefliu Sample sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
5.97 0.32 ug/L 369407 1,4-Dichlorobenzene-d4 9.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3-[1,3]dioxolan-2-y . . . 174 C8H14O4 1000186-02-3 28 2 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 492 (5 970 min)' 08256.D (-488) (-) m/z 73.10 100.00% 73
5000 43 _ 100 5 60 5.80 6.00 6.20 6.40
n/z— > 0- 10 i ""i "" i 20 30 40 lL5 50 87 103 — —nmmmmmmmmmmmmmmm 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.05 25.62%
_X. V.. Abundance #25344 Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5000 IMMAMaP—P—MAa 560 5.80 6.00 6 20 6.40 43 m/z 41.10 10.73% 27 55 , 87 113 131 174 0-PTT --- ■ i ■ ■ 11 r " 'T1 TTgTLTTTTTTTTITTTTTT n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #108252 Pentanol, 5-amino- 31 . J, A l| y, ,, P , 5.60 5 80 6 00 6.20 6.40 5000- m/ z 45.10 9.99%
41 56 67 85 1 03 0^ 1111111111 i'I'i'i '' '‘I.. . ' I' "Iii ■' 1 1 I 1 1 1 1 I 1 1 I 1 I ' 1 1 ' I 1 1 1 1 I I 1 1 1 I 1 1 1 I I I ■' * ’ I i ■1 ■ ■ ।1 ■1 ■ ।1 ■ n/z- > Abundance 10 20 30 40
3b 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #857 N-Ethylformamide M... 5 60 580 600 6.20 6.40 73 m/z 71.00 6.58% 5000 44 58 18
/z— > 0 mH 14——— I ’ ’ " O' 1" i '' ‘' i " " I " ' ' i1' " I " " I' ' " i " " I " ‘' i' " ' i1 " ' i " 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1.......................... 5 60 5 80 6 00 6 20 6 40
08256 .D 041702SCAN.M Thu Apr 18 09:27:13 2002 Page 8
NYC-WTC_000047897
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NYC-WTC_000048378
GCMS analysis report for sample AE08265 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047867
GCMS analysis report for sample AE08255 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047593
Laboratory report documenting GCMS analysis of sample AE07976 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047577
Laboratory report documenting GCMS analysis of sample AE07975 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046771
Laboratory report documenting the GCMS analysis of sample AE08065 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048401
GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047608
Laboratory report documenting GCMS analysis of sample AE07977 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047830
Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046757
Laboratory report documenting the GCMS analysis of sample AE08064 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048436
GCMS analysis report for sample AE08269 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048268
Laboratory report detailing surrogate recovery results for sample AE08260 analyzed on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048421
GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000047744
Department of Environmental Protection GCMS analysis record dated April 8-17, 2002.
Filed in the same folder
NYC-WTC_000047745
Header page for a GCMS data file related to WTC environmental testing in April 2002.
Filed in the same folder
NYC-WTC_000047748
Laboratory report of GCMS calibration data for sample AE08251 conducted on April 17, 2002, listing target compounds and concentrations.
Filed in the same folder
NYC-WTC_000047752
Laboratory report of GCMS reference analysis for sample AE08251 conducted on April 17, 2002, showing recovery percentages for target compounds.
Filed in the same folder
NYC-WTC_000047757
Laboratory report of a GCMS blank analysis for sample AE08251 conducted on April 17, 2002, showing non-detect levels for various compounds.
Filed in the same folder