GCMS analysis results for sample AE08425, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 3-Pentanol, 3-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 6.10 0.40 ug/1 509888 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Dioxolane, 2-heptyl-____________ 172 C10H20O2 004359-57-3 9 Abundance Scan 515 (6.105 min): 08425.D (-509) (-) m/ z 73.10 100.00% 73

5000 40 45 w 5.80 6.00 6.20 6.40 , 11. , 55........ ii , 87 103 I ■ ■ t ■ ■ ■ 1 I ' • ■ ' I • ‘' 1 I > m/z 40.10 26.74% 1 ’ | 1 • ■ 1 i ■ ■ ■ ■ | 1 ' ' ' | 1 WWWWy~Y—WNN -n/z->_______ 10 20 30 40 50 60 70 80 90 100 110 Abundance #114875: 3-Pentanol, 3-methyl- 73

5000 ■ ■ ' i 1 1 1 ' । ‘ ■ 1 ■ । 1 1 1 1 i 1 ' 1 11 5.80 6.00 6.20 6.40 45 55 m/z 43.15 18.85% 87 115 271,32 3,9I I I 50 +. 67, T 1 1 UITt ■ ■ । 1 ' ■ ■ । । ■ ■ | ' l'> । | ... । | । I I I | !

/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #857: N-Ethylformamide 3J 73 A ' 1 " ' I' ' _________ t 1 । । ’ i < » | 5.80 6.00 6.20 6.40 5000 m/z 45.10 10.57%

m/z-> Abundance

5000 , 10131,1125 20 18

30 40 44

50 58

l i > • • » ,■ > • ■ • i > ■ > • i • > • • । 60 #25472: Pentane, 3-methoxy- 70

73 80 90 100 • I > 110 - 5.80 m/ z a.6.00 41.20 6.20 6.40 7.33%

45

29

n/z-> .......... r . . 3940 I , 5050 55.,60 6770pi + 80 10 20 30 ■ ' • | 1 ■ ■ ■ i ■ ■ ■ ■ । ' । । ift 90 101 100 110 5.80 6.00 6.20 6.40

08425.D SCAN020418.M Thu May 02 15:28:08 2002 Page 6

NYC-WTC_000048157