GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial : 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 4 N,N-Diethyl-2-aminoethanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

7.32 0.31 ug/L 341847 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N,N-Diethyl-2-aminoethanol 117 C6H15NO 000100-37-8 91 2 1-Propanamine, N,N-diethyl- 115 C7H17N 004458-31-5 64 3 Methanediamine, N,N,N',N'-tetrae.. 158 C9H22N2 000102-53-4 64 4 Diethylaminoethyl acrylate 171 C9H17NO2 002426-54-2 59 Abundance Scan 721 (7 316 min): 08258.D (-713) (-) m/z 86.10 100.00% 86

5000- 58

42 7.00 7.20 7 40 7.60 0—T ............ .149 , 72 ' I' 1 111'1 " I'' " ‘1111"1' I'' 1 ■ ।11" i11 I 102 117 m/z 58.10 36.52% n/z- > 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #116803: N,N-Diethyl-2-aminoethanol 85

5000 58 1 ,4.9. | 1 i ' ' ' ' i 7 00 7 20 7 40 7 60 m/ z 42.10 12.42% 42 102 117 ..... Ill.... |..... 72....

MN, 01 ■ 11 ■'' 11 >!' 11' ' I " " 111111111 I " 1111111111 1PPP n/Z—> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #34797: 1-Propanamine, N,N-diethyl- 85 A 7 00 7 20 740 7.60 5000- m/ z 56.10 10.71%

K 30 58 100 42 115 15 72

n/z- > Qi - 0 10 20 30 ..50.1 ..... TTT ■1' i'11' i' ■ 1' i 1 ■1' i1'1' i1'1 ■ i' 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #116762: Methanediamine, N.N.N’.N’-tetraethyk 85 7.00 7 20 7 40 7 60 m/ z 40.00 8.93% 5000

30 58 42 4 15 72 99 113 127 157 0 -rrp-r T-p-r TT THmpo ■ । ■1' । ■1 ■ । ’ ■' ■ । ■1 • ।'1 ■ ।'1' । ■ ■ ■ ■ ।■ /z- > 0 10 20 30 40 50) 60 70 80 90 100 110 120 130 140 150 160 7 00 7 20 740 7.60

08258.D 041702SCAN.M Thu Apr 18 09:37:42 2002 Page 9

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