GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020417\08257.D Vial : 15 Acq On : 17 Apr 2002 9:01 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SC7VN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 6 Propane, 1,1-diethoxy- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.71 0.35 ug/L 358877 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 1,1-diethoxy- 132 C7H1602 004744-08-5 16 2 Butanoic acid, 3-hydroxy-, methy... 118 C5H10O3 001487-49-6 10 3 Acetamide, N-(aminocarbonyl)- 102 C3H6N202 000591-07-1 9 4 Silane, dimethyl-60 C2H8Si 001111-74-6 9 Abundance Scan 1129 (9 713 min) 08257 D (-1125) (-) m/z 59.00 100.00% 40 45 59

5000 73 87 103 116 ......... , J, ,w,.,, 9.40 9.60 9 80 1000 0- r( 1 I' 1' ' i 11 r ' i ' 11 ' ■ 11 ।1 ■ 1 ■ । m/z 45.10 87.77% n/z- > 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #113320: Propane, 1,1-diethoxy- 59 47 87 29 103 5000 TT 75 9.40 9.60 9.80 10.00 41 m/z 40.00 82.40% 0- -- ' ' 131 1 1 ' ' ' I n/z— > 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109438 Butanoic acid, 3-hydroxy-, methyl ester 43 74 9.40 960 9.80 10.00 5000 m/z 57.00 75.11% 87 103 ) 59 31 0- 25111 371,1 ■ i ■ ■1 ■ । . . . r| ——r 34189 53 .. 1) .... |'i i . 117 ■ i ■ ■ 1 ’’i ■ ■ ■ ■ । । • । ■ i n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4791: Acetamide. N-(aminocarbonyl)- __ 1 ■ i ■ r ■ ■ i 1 ' 1 1 i 1+II1fIII 43 59 940 9.60 9.80 10.00 m/z 43.05 54.51% 5000- 102 A 74 ------ 0- ■ i ■ ■ ■ ' i ■ ■ ■ ' i ‘ i ' ' ■ ' i ■ ■ ' 1 i ■ ■ ' ■ i ' 1 ' 1 I n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 9.40 9.60 9.80 10 00

08257 .D 041702SCAN.M Thu Apr 18 09:33:57 2002 Page 11

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