GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08257.D Vial : 15 Acq On : 17 Apr 2002 9:01 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 N,N-Diethyl-2-aminoethanol Concentration Rank 7 R. T. EstConc Area Relative to ISTD R.T.

9.66 0.30 ug/L 310468 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N,N-Diethyl-2-aminoethanol 117 C6H15NO 000100-37-8 47 2 N,N-Diethyl-2-aminoethanol 117 C6H15NO 000100-37-8 23 3 2-Fluoroimidazole 86 C3H3FN2 1000129-59-1 9 4 Trimethylamine 59 C3H9N 000075-50-3 9 Abundance Scan 1120 (9 660 min): 08257 D (-1109) (-) m/z 86.10 100.00% 86

5000 40 58 72 AW 47 117 9.40 9.60 9.80 10.00 ! 102 1 n/z-> ol 10 20 30 40 50 160....70 80 90 •' । ’1 100 110 120 m/ z '58.10 58.62% Abundance #116803: N,N-Diethyl-2-aminoethanol 85 MM"k rV 5000 58 940 9 60 9 80 10 00 42 m/z 40.00 55,. 17% 72 102 117 Ol ■ I ' 1 1 1 I ' 1 1 ' I ' 1 ' 1 I 1 I 1 1 1 I '"'I In I ' ' -PPH n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #34626 N,N-Diethyk2-aminoethanol 85 30 9.40 9.60 9.80 10.00 58 5000 m/z 72.00 40.66% 42 15 102 n7 n/z-> 0) 1 1 I ' 1,4: 1 1 I 10 20 1— 4152 30 40 50 66 72 + ' 111 N+...... 60 70 80 90 *1 i < ■ ■ ■ । l ■ ■ • i ■ • 11' i ■ ■ 100 110 120 Abundance #34865: 2-Fluoroimidazole 85 9.40 9 60 ' 9 80 10 00 m/z 41.10 38.22% 5000 59

n/z- > 0 10 20 30 41 40 50 53, .1 60 67 73 r' I ' 1 ' ' I ' ' 70 80 I.................. 90 100 110 120 AuhujhinM“n/in 9.40 9 60 9.80 10.00

08257.D 041702SCAN.M Thu Apr 18 09:33:55 2002 Page 10

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