Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.
NYC-WTC_000022526–000022538Folder label: “GCMS X 5/17/12 A 5/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\11425.D Vial: 11 Acq On : 21 May 2002 6:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.15 12.89 ug/1 1010870 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 2-Pentandne, 4-hydroxy-4 -methyl- 116 C6H12O2 000123-42-2 45 3 2 -Pent anone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 42 4 Acetic acid. 1,1-dimethylethyl e... 116 C6H12O2 000540-88-5 36 Abundance y Scan 523 (6.152 min): 11425.D (-520) (-) m/z 43.10 100.00% 43
5000 59
101 1 1 i UUUIs’ । i । 11 83 | 113 5.80 6.00 6.20 6.40 0 '" i ■ ■ ■ ■ i'1 ■ ■ i'-H#Amm TH 201 m/z 59.10 48.99% mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #109755:2-Pentanone, 4-hydroxy-4-methyl- 43
5000 • > i ■ ■ > • । । ' i > ■ ■ ■ | । । । . 59 5 80 6.00 6.20 6.40 m/z 58.10 20.41% 15 31 101
n/z-> 0 -H 83 ,.............................. 'l" " I" ■ 'I1'1" I' ■ ■111" ■ i" " i" " i" " i" " i ■ • • ■ i"1T1" i" " n "11" " i 10 20 30 40 50 60 70 80 90 100110120130.140150160170180190200 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- 43 IT 7 1*1717 TTBBnm—pr 5.80 6.00 6.20 6.40 5000 m/z 101.10 16.95% 59 101
m/z-> O+ mm huigrigun 69 83 27 1 ■ । | . > > i | i i ■ I | i < i I । I ■ I i | ( । i . । i < i > । .7 ■ I | I 11 I | I I I I | I I I I | U I ■ | I I I I 11 I I I | I I I I |
10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #109756:2-Pentanone, 4-hydroxy-4-methyl- ~*1n,———mTTTTgr 43 580 6.00 6.20 6.40 m/z 41.05 6.73% 5000 59
31 . 0 " ' I " ■' l " . ' ■ Th ' l' it .... । 83 101 | " I " 1111'1 T " | 11111111 > 11111111111111 •> 11111J l-r 1111111 j 1 rrr r i 1 1 r i tSTmoPTTr m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 5.80 6.00 6.20 6.40
11425.D SCAN020521.M Fri May 24 09:26:46 2002 Page 5
NYC-WTC_000022534
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NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022561
Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046192
Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046147
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Calibration verification report listing response factors for target compounds in sample AE11424 analyzed May 17-21, 2002.
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