GCMS results for sample AE11425, May 29, 2002

NYC 9/11 Public Portal Document Llprary search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11425.D Vial: 11 Acq On : 21 May 2002 6:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.45 ug/1 35267 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 72 2 Butanoic acid, 3-oxo-, 2,2,2-tri... 232 C6H7C13O3 058547-15-2 10 3 2,3-Dioxabicyclo\[2.2.2] oct-5-ene. . . 168 C10H16O2 000512-85-6 9 4 N-Acetylpyrrolidone ____________ 127 C6H9NO2 000932-17-2 9 Abundance Scan 518 (6.123 min): 11425.D (-512) (-) m/z 43.05 100.00% 43

5000

* «T * » • ' I * * r . । i tt i । 97 125 5.80 6.00 6.20 6.40 OTT , ul r.k,h .+1 . ................ . m/z 125.00 11.01% m/z-> o 50 100 150 200 250 300 350 400 450 500 Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

5000 ■ ■ ' i • ■ ' ■ i ' ■ ■7 i 1 ■ ■ ■ i ■ ■ ' ■ i 5.80 6.00 6.20 6.40 m/z 127.00 10.65% 15 83 125 O-T *1 r. i f) 1".(0( m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #1068: Butanoic acid, 3-oxo-, 2,2,2-trichloroethyl ester 31 ■ ■ ■ i ■ ' ■ ■ i ' ' ■ ■ i ■ ■ ' ■ I 1 1 ' 1 I 5.80 6.00 6.20 6.40 5000 m/z 97.00 8.65% 85

113 . 153 197 234 0 1 Aw *. Mt it. i 1 ■ ■ ■ i ■ ' iz—> ।o I50 100 150 200 250 300 350 400 450 500 Abundance #7498:2,3-Dioxabicyclo[2.2.2]oct-5-ene, 1-methyl-4-(1-met... 43 5.80 6.00 6.20 6.40 m/z 82.00 8.14% 97 5000 71

n/z-> 0154444/4374,18 . ...... ... i0 50 100 150 200 250 300 350 400 450 500 I.A.44, 5.80' 6.00 ‘ 6.20 ‘ 6.40 ' ‘ ‘

11425.D SCAN020521.M Fri May 24 09:26:46 2002 Page 4

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