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GCMS analysis results for sample AE11278, May 2002

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Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024692–000024705

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Library aearen compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Quinazoline, 6-nitro- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 22.30 0.22 ug/1 21508 Acenaphthene-dl 0 24.46 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Quinazoline, 6-nitro- 175 C8H5N302 007556-95-8 16 2 Benzamide, 2,6-dichloro- 189 C7H5C12N0 002008-58-4 12 3 1,2,B-Thiadiazole, 4-phenyl- 162 C8H6N2S 025445-77-6 10 4 Benzamide, 2,6-dichloro- 189 C7H5C12NO 002008-58-4 10 Abundance Scan 3271 (22.298 min): 11278.D (-3261) (-) m/z 173.00 100.00% 173 102

5000 75 137 210 44 63 85

mfe-> .. I ■ i ■"' । ■ 11i ■" i' bu 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 22.00 22.20 22.40 22.60 m/z 102.10 80.25% Abundance #75796: Quinazoline, 6-nitro- 175 102

5000 75 129 145 22.00 22.20 22.40 22.60 90 117 m/z 175.00 76.13%

m/z-> 'I "111"1' 11'111'*111'11' I Ju"i....... 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 159 prtTTTT '111" 11" " I" " I" 1

Abundance #125013: Benzamide, 2,6-dichloro- 173 ...... I!I..... 22.00 22.20 22.40 22.60 5000 m/z 210.00 47.84% 74 189 44 109 145

n/z-> ..... 'i-i''I"1 84 93.44++ L ■I" "i" ■ ‘i111 pi111 'i1"111 1gTT 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 4 Abundance #44297:1 2,3-Thiadiazole, 4-phenyl- 102 22.00 22.20 22.40 22.60 m/z 137.10 43.52%

5000 51 63 90 134 ,1 174 TTTT Hla — ’ ’) ..... l|........ 162..................... 'I " "I ' 1.................. । << i । I >> । । । । । । !< I > I | i i i i | i | " | I i | i ' ' I ' ' ' ' I v■ । । । > 1 i । . m/z—> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 22.00 22.20 22.40 22.60

11278.D SCAN020507.M Thu May 16 09:56:21 2002 Page 5

NYC-WTC_000024700

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NYC-WTC_000024700Source: NYC Law Department, mirrored locally

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