Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.
NYC-WTC_000024692–000024705Folder label: “GCMS X 5/13/02 A 5/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library bearen compound Report
Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 15.47 0.68 ug/1 63832 Naphthalene-d8 16.53
Hit# of Tentative ID 5 MW MolForm CAS# Qual J1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 3 3,4 ihydroxybenzyl alcohol, tris .. . 356 C16H3203Si3 068595-79-9 40 4 Benzeneacetic acid, .alpha.,4-bi... 326 C15H26O4Si2 055334-40-2 25 Abundance Scan 2108 (15.465 min): 11278.D (-2094) (-) m/ z 73.10 100.00% 73
5000 267 355 --- 45 15.20 15.40 15.60 15.80 118 154 191 - —hTmuummuTm 251 । 11—00’0171111111117 ... 3233391 m/z 267.00 40.33% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73
355 267 V 5000 ■ ■ i > ■ r‘I741‘1II 15.20 15.40 15.60 15.80 m/z 355.10 33.94% 45 191207223 251 j 323339 | I '1 11 " ' I r‘' "’l'' 111 " 1 TDTUITTTTTT I ’ H 11'11' l1' *11''111 ‘11 ’ I " '11111111 “ 1!1 " 1 11 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 . .......400 15.20 15.40 15.60 15.80 5000 267 m/ z 268.10 11.24% 355 45 28 .1 1 | 96 115133149165 , 193 223 251 | 307323339 TI ‘TmOngT—mTmummhim I i" ■■ 1" ‘11 ■1 mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #27659:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73 15.20 15.40 15.60 15.80 m/ z 356.10 10.00% 267 5000 179 356 45 147 I 28 T —H I 209 ri 'I"" f"1 '1 237 , 11" i" " i ‘ " 111 TIT’ 312 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 15.20 15.40 15.60 15.80
11278.D SCAN020507.M Thu May 16 09:56:20 2002 Page 4
NYC-WTC_000024699
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NYC-WTC_000024706
Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024730
Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024871
Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025580
GCMS analysis report for sample AE11568 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024915
Laboratory report of GCMS analysis for sample AE10301 conducted on May 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000024623
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000024624
Laboratory report documenting GCMS analysis of sample AE11305 conducted on May 28, 2002, including surrogate recovery data.
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NYC-WTC_000024629
Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
Filed in the same folder
NYC-WTC_000024640
Laboratory report displaying calibration data for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
Filed in the same folder
NYC-WTC_000024644
Laboratory report displaying reference standard results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
Filed in the same folder