GCMS analysis results for sample AE11155, May 2002

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Data File : C:\MSDCHEM\l\DATA\020515\11155.D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 2-Dodecanol, 2-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 5.25 3.11 ug/1 233861 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Dodecanol, 2-methyl- 200 C13H280 001653-37-8 38 2 3-Pentanol 88 C5H120 000584-02-1 36 3 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 36 4 Aceramide 59 C2H5NO 000060-35-5 9 Abundance' Scan 369 (5.247 min): 11155.D (-363) (-) m/ z 59.10 100.00% 59

5000 43

1 1 1 ■ i ■ 1 i ' 1 ITIT" । ] i i । 69 107 5.00 5.20 5.40 5.60 ■.| ■ 1m — v17 ................... 216 m/z 43.10 43.25% mtz-> 20 40 I60 80 100 120 140 160 180 200 220 Abundance #19343:2-Dodecanol, 2-methyl- 53

5000 5.00 5.20 5.40 5.60 m/z 41.15 13.63% 20 41 2 1 . 1 68 . 83 97 111 125. 140 154 167 ,185 .......... m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #19296: 3-Pentanol 59 — =ermfPr 5.00 5.20 5.40 5.60 5000 31 m/z 107.00 12.58% 41

miz-> 1520——40 171 87 ' I • ■ ■ ' i 1 ■ 1 ■ i ■ ■ ■ ■ i ’ 1 ■ ' i ■ ■ ■ ' i ‘ 60 80 100 120 140 160 ■ i 1 ' 180 ■ i 200 ' ■ ■ ' i ■ 220 Abundance 59 #113152:2-Propanol, 2-methyl- - . . . , Ar 5.00 5.20 5.40 5.60 m/z 69.10 6.96% 5000 31 41 — . 15 , — TTuT — /z—> 20 40 60 80 100 120 140 160 180 200 220 5.00 5.20 5.40 5.60

11155.D SCAN020507.M Thu May 16 09:34:56 2002 Page 6

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