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GCMS analysis results, sample AE07516, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE07516 conducted on April 11, 2002.

NYC-WTC_000047389–000047401

Folder label: “GCMS X 4/2/02 A 4/4/02

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Scanned page image, NYC-WTC_000047395
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07516.D Vial: 12 Acq On 4 Apr 2002 5:13 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHODS\SC7kN02 04 03.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Furan, 2,5-dihydro-3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.27 0.14 ug/1 105444 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, 2,5-dihydro-3-methyl- 84 C5H8O 001708-31-2 4 2 2-Butyne-l,4-diol 86 C4H602 000110-65-6 3 3 Thiophene 84 C4H4S 000110-02-1 2 4 Thiophene 84 C4H4S 000110-02-1 2 Abundance Scan 33 (3.273 min): 07516.D (-22) (-) m/z 84.00 100.00% 49 84

5000 WAt 11 111' 1 11 1'1 ■ r 1 " i1 1 ■11' 1' ■ i11' 3.20 3.30 3.40 3.50 3.60 3.70 o1 Th 1 r 111111" i" " i" " r ■" i" " r1" r " ’ i' i" " r "11" " r "' i" " r " "11" " i" m/z 49.10 87.78% m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 / Abundance #386: Furan, 2,5-dihydro-3-methyl- 23 41 84 69 5000 56 ■1 r 1 '' r 1 1 ■ r 1 11 r 1'11 •''11' ■ 3.20 3.30 3.40 3.50 3.60 3.70 51 m/z 47.10 64.65% 15

m/z-> 0- 0 2 । 19 25 TTHTH Hr llule.u 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 , 61 65 , 73 77 TTT TTnTT Imp Abundance #108388: 2-Butyne-1,4-diol 29 33 57 1 ■ 111 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 86.00 43.65%

25 43 51 68 A/MMwhmn. m/z-> 01 0 i"" r "‘I" " i" ... 1 /1.34 4,471 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1.1. 1 173,77.81.s.. Abundance #33732: Thiophene 84 3.20 3.30 3.40 3.50 3.60 3.70 58 m/z51.00 32.03% 45 5000 MM, 39

50 i 0 1 12 ......................... "'I' 26 32 , I ■ 11111111111111111111111 HHrmt 1 . 1.. 89,11)188,, ‘ T ‘ I‘ /z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70

NYC-WTC_000047395

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NYC-WTC_000047395Source: NYC Law Department, mirrored locally

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