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GCMS analysis results for sample AE07632, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE07632 conducted on April 9, 2002.

NYC-WTC_000047277–000047287

Folder label: “GCMS X 4/2/02 A 4/3/02

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Scanned page image, NYC-WTC_000047283
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020403\07631.D Vial: 21 Acq On 4 Apr 2002 3:35 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Furan, 2,5-dihydro-3-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.29 0.42 ug/1 224592 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1- Furan, 2,5-dihydro-3 -methyl- 84 C5H80 001708-31-2 4 2 2-Butyne-1,4-diol 86 C4H602 000110-65-6 3 3 Thiophene 84 C4H4S 000110-02-1 2 4 Thiophene 84 C4H4S 000110-02-1 2 Abundance Scan 35 (3.285 min): 07631.D (-19) (-) m/z 49.10 100.00% 49 84

5000

TII’ 1 1 1 1 1 I ' I [ ' 1 1 1 I 17 1 I I I I I I I I I I 3.20 3.30 3.40 3.50 3.60 3.70 01 TTp-rTrp-rTTp-rrTp-rrrp-rrTp-rTT-^^ 11 । t r 11 । । < । । । j r 11 । । । ^ 11 । । । I""!1 ^m/z^^ m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #386: Furan, 2,5-dihydro-3-methyl- 29 41 84 69 5000 56 '11 I'11 ■ r 1 11 r ''11 1 111 11111111 53 3.20 3 30 3.40 3.50 3.60 3.70 15 26 m/z 86.00 48.79% / Tl/Z-> o1 2 TTTTT 171/.,19... , 61 65 , 73 77 81 Tut 4 I I I I rJ I I I I I I I 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 11"11" 11 r

Abundance #108388: 2-Butyne-1,4-diol 29 39 57

3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 47.00 43.02%

01 T-rrrp-r 26

1,34 1474 43 51

1111111171 68

1111 77 81 85 ' r " ■ r "' 111" i " ‘ ■ r /W MVMwwya i"111 miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116585: Thiophene 84 3.20 3 30 3.40 3.50 3.60 3.70 m/ z 51.05 29.83% 5000 45 58 PMApu 39

m/z-> 0 ■ ।" " ।1 0 5 12 18 26 32 „ 1"111''' i'1''111'1111111111 111'1 Tt 50.. lls.. 69....76..31 T 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1I0000‘0‘T000umVuTprr 3.20 3.30 3.40 3.50 3.60 3.70

07631.D SCAN020403 .M Thu Apr 04 10:49:27 2002 Page 3

NYC-WTC_000047283

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NYC-WTC_000047283Source: NYC Law Department, mirrored locally

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