Laboratory report documenting GCMS analysis of environmental sample AE07628 conducted on April 9, 2002.
NYC-WTC_000047245–000047255Folder label: “GCMS X 4/2/02 A 4/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\020403\07628.D Vial : 19 Acq On 4 Apr 2002 1:43 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 2-Butyne-1,4-diol Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 3.27 0.14 ug/1 92108 1,4-Dichlorobenzene-d4 10.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butyne-1,4-diol 86 C4H602 000110-65-6 3 2 Thiophene 84 C4H4S 000110-02-1 2 3 Thiophene 84 C4H4S 000110-02-1 2 4 Furan, 2,5-dihydro-3-methyl-______ 84 C5H80 001708-31-2 2 Abundance Scan 32 (3.267 min): 07628. D (-21) (-) m/z .49.10 100.00% 49 84
5000
'' ■ I • ■' 11 ■ ■ ’ ■ I ■ ■1 -1'11111'1 > 1111 3.20 3.30 3.40 3.50 3.60 3.70
w/"uhss m/z 84.00 93.94% 0- TTTTYrTTTpnnnyrTTTpnnTpTTnTT^^ 1’11 '" r "' r ■ n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108388: 2-Butyne-1,4-diol 29 33 57
5000 68 3.20 3.30 3.40 3.50 3.60 3.70 43 51 m/ z 47.00 60.94% 0 '1" r'" i" " i 21.34 4.47 1 61 ,73 77 81 85 11 TTUuun I ■ 11 ■ 1111H1111111 WVMM m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116585: Thiophene 84 i ■1 ■ ■ i T-
3.20 3.30 3.40 3.50 3.60 3.70 58 5000 m/z 86.00 53.25% 45
o1 "" | | 12 18 26 32 39
|1" 11 ■ > r > 11 • " |11" | ■ 11 > |111! | >! l» 50 thHm . +F476.8Q17 T-rp-r w/"y"ymiiy m/z- > 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33732: Thiophene 84 3.20 3.30 3 40 3.50 3.60 3.70 m/z 51.00 43.22% 58
5000 39 45 AWHyMuaLow 1 12 26 32 50 | 69 80 0 11" i'1" r "11 ’111 r ■ ‘r r । i| 11111111,1111 111 1 tl1111111 ll I 1111111111111111111M1I 1188,1111111 m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70
07628.D SCAN020403.M Thu Apr 04 10:36:25 2002 Page 3
NYC-WTC_000047251
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NYC-WTC_000047452
Technical documentation listing GC/MS method parameters and internal standard data for analysis performed in early April 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047463
Laboratory report detailing GCMS analysis of sample AE07768 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047216
Laboratory results for unknown compounds and surrogate recovery in sample AE07569 analyzed on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047389
Laboratory report documenting GCMS analysis of environmental sample AE07516 conducted on April 11, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047333
Laboratory report documenting GCMS analysis of environmental sample AE07511 conducted on April 11, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047377
Laboratory report documenting GCMS analysis of environmental sample AE07515 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047402
Laboratory report documenting GCMS analysis of environmental sample AE07518 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047256
Laboratory report documenting GCMS analysis of environmental sample AE07630 conducted on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047277
Laboratory report documenting GCMS analysis of environmental sample AE07632 conducted on April 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047355
Laboratory report documenting GCMS analysis of environmental sample AE07513 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047493
Laboratory report detailing GCMS analysis of sample AE07772 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047344
Laboratory report documenting GCMS analysis of environmental sample AE07512 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000047156
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated April 2-3 2002.
Filed in the same folder
NYC-WTC_000047157
Header page from a DEP laboratory data file containing sample identification and processing metadata from early April 2002.
Filed in the same folder
NYC-WTC_000047159
Laboratory results for volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.
Filed in the same folder
NYC-WTC_000047177
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.
Filed in the same folder
NYC-WTC_000047181
Calibration data report for GCMS analysis of volatile organic compounds performed on April 2-3, 2002.
Filed in the same folder