GCMS analysis results, sample AE07518, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020404\07518.D Vial: 14 Acq On 4 Apr 2002 7:05 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Ethyl Chloride Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

3.31 0.56 ug/1 374253 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 4 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 4 3 Formic acid, ethyl ester 74 C3H602 000109-94-4 3 4 Formic acid, ethyl ester 74 C3H602 000109-94-4 3 Abundance Scan 39 (3.308 min): 07518.D (-21) (-) m/z 49.10 100.00% 43 74 84

5000 35

TTItrTt1—111100B6—101ITTTTTTIIIT 3.20 3.30 3.40 3.50 3.60 3.70

m/z-> Of ' ' i ' ■ ■ ' i 1 ■ ' ' i ■ 10 20 30 H 40 50 ■ i ■ ■ ■ ■ i ■ 60 70 TIl 80 "TI‘ > > । 11 । 11 । । । । । । 90 100 110 m/ z 74.00 96.48% • Abundance #107943: Ethyl Chloride ??

64 5000 1' i1 ■1' I '11 " 1' i ■ ■ ■ ■ i' ■ " i' " ' i 3.20 3.30 3.40 3.50 3.60 3.70 49 m/z84.00 94.11% 35 0 I-" 111+I ^7-‘15 +l, '' ''n1' '' * Il ■ । ■ ■ ■ ■ । 1 ■ ■ ■ । ■ ■ ■ ' । ■1 1 । ■ ■ ■ ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 714 ■' ।1 ■ ■111'11111 ■1 rri ■ ■ ।11 > 111 ■ ■ 11 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/ z 47.00 :76.30% 47 35 — /z-> Of 12 > ■ i 1 ■ ■ ■ । ■ 10 20I 26,1 30 40 Hl ■ ■ ■. ........... ' 50 60 70 80 . 108 i • । • > > > । ■ • ■ • i ■ ■ • ■ । 90 100 110 Abundance #108297: Formic acid, ethyl ester 31 3.20 3.30 3.40 3.50 3.60 3.70 m/z 82.00 50.85% 5000 45

m/z-> 0 1 1 I 1 1 1 1 I 1 1 10 20 — 301 -9157 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

NYC-WTC_000047408