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GCMS analysis results for sample AE01142, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01142.D Vial: 8 Acq On : 25 Feb 2002 5:01 pm Operator: • ' Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 8 4-Cyanocyclohexene $$ 3-Cyc... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

9.96 0.06 ug/L 26666 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Cyanocyclohexene $$ 3-Cyclohex. .. 107 C7H9N 000100-45-8 91 2 3-Cyclohexene-l-carbonitrile $$ ... 107 C7H9N 000100-45-8 80 3 3-Cyclohexene-l-carbonitrile $$ ... 107 C7H9N 000100-45-8 9 4 2-Penten-4-yne, 2-methyl-__________ 80 C6H8 000000-00-0 9 Abundance Scan 583 (9.955 min): 01142. D (-) m/z 54.10 100.00% 54

5000 41 80 107 67 92 9.60 9.80 10.00 10.20 0- ■ ' i ' ' 1 ' i ‘ 1 ■ ‘ i ‘ ‘ i ■ 1 ' ' i' TFP3T ■ । 1 ■ m/ z 80.00 46.18% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #10984: 4-Cyanocyclohexene $$ 3-Cyclohexene-1-carbonitrile... 54 39

5000 27 79 0 107 9.60 9.80 10.00 10.20 67 m/ z 79.00 42.53% 92

0- ■ ' i ‘ 1 ■ ■ i • ' 1 ■ i ' ■ ■ ' i 1 ■ ■ ■ i 1 .......I 1 । 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #10985: 3-Cyclohexene-1 -carbonitrile $$ 3-Cyclohexenyl cya... 54 9.60 9.80 10.00 10.20 39 5000 m/ z 41.10 42.41% 27 80 67 107 92 49 I ....Il..... . 01 1 1 1 1 ‘ 1 1 I ' 1 ' ‘ 1 1 ' 11I 1 1 ' 1 1 i 1 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #10988: 3-Cyclohexene-1-carbonitrile $$ 3-Cyclohexenyl cya... 31 9.60 9.80 10.00 10.20 m/z 107.10 41.34%

5000

15 39 , 58 79 107 0 1I01I0*VV**02* n/z-> 10 20 30 40 50 60 70 80 90 100 110 9.60 9.80 10.00 10.20

01142 .D HP022102.M Tue Feb 26 08:30:35 2002 Page 10

NYC-WTC_000003536

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NYC-WTC_000003536Source: NYC Law Department, mirrored locally

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