GCMS results for sample AE00699, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00699.D vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************* * * * * * * * * ****** Peak Number 4 2-Cyclobutylprop-2-en-l-ol ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.84 0.20 ug/L 63829 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 2-Cyclobutylprop-2-en-l-ol $$ Cy... 112 C7H120 116203-80-6 53 2 2-Pentenal, (E)- (CAS) $$ E-2-pe... 84 C5H8O 001576-87-0 53 3 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H80 000107-86-8 53 4 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H80 000107-86-8 53 Abundance Scan 128 (4.835 min): 00699.D (-) m/z 84.00 100.00%| 56 84

41 5000

n/z-> Abundance O+ " i" " i" " r' "i1 ■ + 49 i" " r ■" i1'" r1 ■ ■ i — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 #13626: 2-Cyclobutylprop-2-en-1-ol $$ Cyclobutaneethanol,... 4.40 m/z 4.60 55.10 4.80 5.00 5.20 95.93%

56 84

5000 —."71 4.40 460 4.80 5.00 5.20 41 69 79 m/ z 59.10 79.27%

m/z-> O+ " i" " i ■ ■" i" " i1" IEnTi m 112 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 i11" " i" 1111"' r1 ■■ i

Abundance #3202: 2Pentenal,,5) (CAS) $$ E-2-pentenal $$ PENTENAL ...

39 83 —A 4.40 4.60 4.80 5.00 5.20 5000 m/z 83.10 73.43% 50 69

01 T mHH fm । । । ■ l ■ ■" p • ■ ‘ I T’ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3221:2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal $$... ’ • i। i < ■ ■ i■ ■ > > । ' i < ■ 84 4.40 4.60 4.80 5.00 5.20 55 m/z 41.10 55.37% 39 5000 27

44 69 0 " r " • r ..... . m11 m mmkmpm 1’"’ i • ■ 1 11 ■ ' ’ ■ i ■ 1 ■ 1 i ' ■ ■ ■ i ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 4.40 4.60 4.80 5.00 5.20

00699 .D SCAN508 .M Thu Jan 17 08:17:00 2002 Page 6

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