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GCMS blank analysis results for sample AE03184, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting a GCMS blank test for sample AE03184 conducted on March 6, 2002.

NYC-WTC_000006026–000006044

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006033
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR01\0212B.D Vial: I Acq On 1 Mar 2002 10:18 am Operator: Sample : lab blank 2/12 Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Cyclobutaneethanol, beta.- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 4.01 0.06 ug/L 27411 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclobutaneethanol, .beta.-methy... 112 C7H12O 116203-80-6 9 2 2-Butenal, 2-methyl- (CAS) $$ 2-... 84 C5H80 001115-11-3 7 3 2-Butenal, 2-methyl- (CAS) $$ 2-... 84 C5H80 001115-11-3 7 4 2-Butenal, 2-methyl- $$ Crotonal... 84 C5H80 001115-11-3 7 Abundance Scan 56 (4.006 min): 0212B.D (-) m/z 55.00 100.00% 55 84

5000

41 ......... A.........

Ci, 3.60 3.80 4.00 4.20 4.40 0 IItft. I Hmm r "' i" " ।" i" " i" " r111 r "11 m/z 84.00 89.32% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #13627: Cyclobutaneethanol, .beta.-methylene- 55 84

5000 3.60 3.80 4.00 4.20 4.40 41 69 79 m/z 51.00 24.83% 112 O+ TF’T r'" 111" r 1" I" " I" " 111'' 11" 11 \ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3220: 2-Butenal, 2-methyl- (CAS) $$ 2-FORMYL-2-BUTENE $$ ... 55 84 29 4 3.60 3.80 4.00 4.20 4.40 5000 m/z 41.10 23.62% 39

0- TrmTrn- T‘———1——0TT—T11—571"15 pTTTrrrrTpnn-rpnT-rY^^ mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3214:2-Butenal, 2-methyl- (CAS) $$ 2-FORMYL-2-BUTENE $$ ... 23 55 3.60 3.80 4.00 4.20 4.40 m/z 53.00 17.38% 39 84 5000

50

m/z-> 0 i" " i'11 L I" " r " 1 r ■" i" " r "' i" " ir 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 3.60 3.80 4.00 4.20 4.40

212B.D HP022102.M Mon Mar 04 12:32:45 2002 Page 5

NYC-WTC_000006033

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NYC-WTC_000006033Source: NYC Law Department, mirrored locally

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