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GCMS blank analysis results for sample AE03184, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting a GCMS blank test for sample AE03184 conducted on March 6, 2002.

NYC-WTC_000006026–000006044

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006032
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document ulprary searcn compound Keporc

Data File : C:\MSDCHEM\1\5973N\02MAR01\0212B.D Vial: l Acq On : 1 Mar 2002 10:18 am Operator: Sample : lab blank 2/12 Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 ISOBUTYRALDEHYDE, DIMETHYLA... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.93 0.06 ug/L 25994 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H1402 000000-00-0 56 2 Propane, 1,l-dimethoxy-2-methyl- 118 C6H1402 041632-89-7 56 3 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H14O2 000000-00-0 56 4 Propane, 1,l-dimethoxy-2-methyl-... 118 C6H14O2 041632-89-7 56 Abundance Scan 49 (3.927 min): 0212B.D (-) m/z 75.00 100.00% 75

5000 87 55 41 47 51 71 84 3.60 3.80 4.00 4.20 0 ............ ..... ...... mm -H .......... —+L |,J TT 111 ’+’’’411’111 ITTT’l " ‘ । | 1 1 1 1 | t 1 1 1 | "I’t m/z 87.10 40.29% n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #17847: ISOBUTYRALDEHYDE, DIMETHYLACETAL $$ 1 1-Dimethoxyi... 75

5000 87 3.60 3.80 4.00 4.20 47 55 m/z 55.00 30.29% 31 --43 59 7,1 Of "It HTTTTT — * n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #17846: Propane, 1,1-dimethoxy-2-methyl- 75 -A— 1I 3.60 3.80 4.00 4.20 5000 m/ z 47.10 17.24% 87 55 31 ,2 47 m/z-> 5 0b ■ i'" ■ i" " i ■1" 11" . 43+4. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 59 71 TTHITTTT — TTIPg

Abundance #17848: ISOBUTYRALDEHYDE, DIMETHYLACETAL $$ 1 1-Dimethoxyi... I 1 1 ' 1 I ■ ' ' 1 I 75 3.60 3.80 4.00 4.20 m/ z 41.10 14.08%

5000 87 15 55 27 31 47

/z-> 0b LL TH-H 1'" i1 ■1T 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 59 71

3.60 3.80 4.00 4.20

)212B.D HP022102.M Mon Mar 04 12:32:44 2002 Page 4

NYC-WTC_000006032

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NYC-WTC_000006032Source: NYC Law Department, mirrored locally

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