GCMS results for sample AE00699, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00699.D Vial: 4 Acq On : 16 Jan 2002 1:20 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.49 0.11 ug/L 33887 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro­ 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 56 4 lH-Pyrazole, 1-methyl- (CAS) $$ ... 82 C4H6N2 000930-36-9 9 Abundance Scan 10 (3.488 min): 00699.D (-) m/z 74.00 100.00% 7l4

82 5000 47 ■ > i < ■ ■ 11 ■ > ■ ■ i ■ > • ■ i ■ ■ ■ ■ l • ■ 39 3.50 3.60 3.70 3.80 3.90 Of ........I. ,1.1..... TIt m/ z 81.90 61.42% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35

5000 82 3.50 3.60 3.70 3.80 3.90 47 m/z 76.00 34.85%

Of ’-TT^T r /‘‘‘11I — ‘I**II TUI 1 1 i 1 1 '■■■ । 1 ' ' ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 7l4

3.50 3.60 3.70 3.80 3.90 5000 82 m/z 47.10 27.77% 47 35 .................. ......hi,.. MI-Pa J l........ -199 . m/z-> 01

Abundance 10 20 30 40 50 60 70 80 Tdil 90 100 #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 110 ‘IT AA.N 4 3 50 3.60 3.70 3.80 3.90 82 27.13% m/z 83.90

5000 47 35 12 0 —PTTT 4 lvoi.. ri TU1 108 1 I 1 1 1 ' I ■ 1 ' 1 I ‘ ' mlz-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

30699.D SCAN508.M Thu Jan 17 08:17:00 2002 Page 3

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