GCMS analysis results for sample AE00165, Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB04\00165.D Vial: 4 Acq On : 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.09 ug/L 41240 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW Mol Form . CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 38 Abundance Scan 10 (3.488 min): 00165.D (-) m/z 74.00 100.00% 74 82 5000 47 / 3.50 3.60 3.70 3.80 3.90

niz-> Of —.—.4. p 1 10 20 30 40 50 60 70 Tnit 80 *1***I**’*!’ SO 100 110 m/z 82.00 53.57% Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 Al i ■ ■ ■ ‘ i1 ■ ■ ■ i' ■ ■ • i 3.50 3.60 3.70 3.80 3.90 47 m/z 76.00 34.43%

niz-> 0! Abundance m10 20 30 35

40 50 60 _________ L ‘ f‘ IT* i ' 70 80 TUB 90 Ipps 199 100 110 —■ #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 1 3.50 3.60 3.70 3.80 390 5000 m/z 47.00 28.09% 47 35 12 — 1 108 Of - ' I ‘ ‘ ‘ ’ I ‘ ‘Lit TPPPITT miz—> 10 20 30 40 50 60 70 80 90 100 110 ...N....... M... Abundance

35 #11644: Acetonitrile, dichloro- 74 5135.4222" 3.50 3.60 3.70 3.80 3.90

5000 82

47 AAN 0 II**PEIAg I ' 1 I)ni i । । । । i i । । 1 1 1 1 1 1 ■ i ■ ■ ■ ■ i ■ ■ ■11 ■ ■' ■ । ■ ■ ‘ ■ ।1 ■1 ’ i ■ ■ ■ ‘ i1 r miz-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

0165.D SCAN508.M Tue Feb 05 09:47:33 2002 Page 3

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