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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
Document / 19 pages

GCMS blank analysis for sample AE00555, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 3-METHYLBENZOTRIAZOLE N-OXI.. Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 24.85 0.05 ug/L 35251 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm ■ CAS# Qual

1 3-METHYLBENZOTRIAZOLE N-OXIDE $$... 149 C7H7N3O 026198-26-5 9 2 5,6-INDOLEDIOL 149 C8H7NO2 000000-00-0 4 3 Benzaldehyde, 4-(dimethylamino) -... 149 C9H11NO 000100-10-7 4 4 Pyridine, pentamethyl-149 C10H15N 003748-83-2 4 Abundance Scan 1881 (24.849 min): 0109B.D (-) m/z 149.00 100.00% 149

5000

41 49 57 TTT I' 'L |**‘I‘* 24.60 24.80 25.00 25.20 TI-Pmmmmmmmt - m/z 150.00 11.00% i ■ ' ' ' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45028: 3-METHYLBENZOTRIAZOLE N-OXIDE $$ 1H-Benzotriazole,... 149

5000 51 ■ ■ i ■ ' 1 1 i ■ ■ i ’ ■ ■ ' i ■ ■ 78 24.60 24.80 25.00 25.20 m/z 41.10 7.76%

n/z-> 20 30 40 +.. 50 60 65 90 -= 104 119 70 80 90 100 110 120 130 140 150 Abundance #45075: 5,6-INDOLEDIOL 149 ■ ' i ' ■ ■ 1 i ' 'I.......... ... 24.60 24.80 25.00 25.20 5000 103 m/z 57.10 6.56%

50 65 76 92 120 27 lz-> 20 - ' i 1 1 ■ ■ i 1 1 1 1 1 1 30 40 50 60 70 80 p.... +......190 --- 100 110 120 130 140 150 Abundance #45228: Benzaldehyde, 4-(dimethylamino)- (CAS) $$ p-Dimeth... ■ । 1 ■ 1 ' i ' 1 ' 'I 149 24 60 24.80 25.00 25.20 m/z 44.00 5.10%

5000 V Si V 77 ____________42| 51| 61 . 105 118 132 TIUPTTTTTTTTPTTTTI ' I ' t 1 ' I ' ' ' ’ I ' - 1’ I | T II IV! , J 1 , - 11 1'11 1 1 1 1 i ' • ■ ‘I m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 24.60 24.80 25.00 25.20

109B.D SCAN508.M Wed Jan 30 09:02:34 2002 Page 14

NYC-WTC_000051528

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NYC-WTC_000051528Source: NYC Law Department, mirrored locally

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