GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.29 ug/L 372732 Phenanthrene -dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 93 2 Anthracene-D10 188 C14D10 000000-00-0 90 3 Anthracene-dlO- 188 C14D10 001719-06-8 87 45-methyl-2-oxatricyclo[6.5.0.0(4...188C13H160 Abundance 000000-00-0 64 Scan 1699 (22.771 min): 30644A.D (-) m/z 188.10 100.00% 188

5000

94 80 22.40 22.60 22.80 23.00 23.20

miz-> 42 54 66 --1801 160 106 118 . 1 — 136 146• 01 111111 " 1" 111 ■'1 ■ i ■ ■11'1" " 11 " 111T' । " ■ 111', 11111, । " । ■ । 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TI m/ z 94.10 21.70% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 184.10 16.29% 66 . 158 miz-> 0- ‘ r ■' ■ i11 ■ ■ i' ■ I' i1 11" H " ।" । ■ । ■" 1111" ।u 111"1 ■ ।111H1"1111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 sl.. Abundance #84498: Anthracene-D10 188 ' i ■ ■ ■ ■ i ■ 1ntI । । ' । I । । । । I 1 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.15 15.21% 80 94 66 160 । 0- —mPTP ' I I ' I I I " I " I rrrm rmr I vr I I | ! 1 ! |1 I I I |'l I I I | I I I ! | rltlll I 1 "11 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ■ i 1 ' ■ ' । ■ TT M । 1 i 1 1 । । i । 188 22.40 22.60 22.80 23.00 23.20 m/z80.10 13.54% 5000-

160

iz-> 66 0 1 ■ i11 ■11" 111" ।' i1" 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 III........ U 22.40 22.60 22.80 23.00 23.20

30644A.D SCAN508.M Fri Feb 22 11:44:25 2002 Page 14

NYC-WTC_000004913

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