GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 * Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.18 ug/L 227937 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 4 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 53 Abundance Scan 1656 (22.280 min): 30644A.D (-) m/z 192.10 100.00% 1'12

5000

146 160 ■ 1 । r ' ■ ‘ i ' '

42 52 70 82 96 120 , 22.00 22.20 22.40 22.60 0 TTTTTTTTTT+++ 1 1 rrt] Il I ! | I I I I | I 1TI | m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 — 1 ''I..... . m/z 191.00 15.92%

Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 A 22.00 22.20 22.40 22.60 146 175 m/z 146.10 15.04%

0 1111116111"’1EEII0BT071Tm111111111011 1111 ■ ■ i ■ ■'111 1 p..... Tumpu n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 . .....A.... /.I 22.00 22.20 22.40 22.60 5000 m/ z 96.00 14.21%

165 91 103 119 131 147 n/z—> 0 .........................................................। li ■' i1" ■ i111' i " " i" " r 1111" ■ 'i1 ■ " । i______ |_____ U______I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । । <।*>>>।•>■■[ | 1 1 47 i 7r ' " 1 Hm "'1

Abundance #88409: N-perdeuteriobenzylideneaniline ■ • i ■ ■ ■ ■ i ■ ■ 19 2 22.00 22.20 22.40 22.60 m/z 193.10 13.82%

5000 82

54 110 30 I 94 160 0 I I........... ’ 1’4’11’ -H rl " " I" " I " " 11" 11'" " I " " I" 'I1 Tammn - n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22,00 22.20 22.40 22.60

30644A.D SCAN508.M Fri Feb 22 11:44:25 2002 Page 13

NYC-WTC_000004912

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