DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02016.D Vial: 4 Acq On : 26 Feb 2002 12:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 111826 Phenanthrene-dl0 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 47 Abundance Scan 1675 (22.283 min): 02016.D (-) m/z 192.00 100.00% 192

5000

96 146 160

m/z-> 0 1 1 I ' 1 ' ' I 44 '1 1 1 I‘ — 82 . I i 118 ' I 1 1 1 1 | ' I | i | I I n । i I I i | | i i 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 . + TH 4— 22.00 22.20 22.40 22.60 m/ Z 96.00 16.64% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.00 15.62%

m/z-> 0 " i " 11 r ■ ■' i " ■' i " " i " " i1" 11" " r 1 । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■111 ■111 *1 ■111 ■ ' i " ‘ ■ i " " i' '''I ""I1 I Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 .......M..... M 22.00 22.20 22.40 22.60 5000- m/z 146.10 15.26%

165 91 103 i 119 131 147 177 0 mAmt + । li____ ।______ |_____ H______ [______ , " i " " I " " i' " ■ i " ‘11 " " 11' m ' ■ ■ ■ ।, i 111 ■1111 *1 *1 r11111 > * ri 1111 j p pi j 11 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140150160170 180190200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ’ I’’ -...... 8r 22.00 22.20 22.40 22.60 m/z 193.10 14.01% 5000 82

54 110 30 1 94 160 0 — i " 111' '' i " " i ■ " 1 1' । " I' 11' I " 1 TTUTTTTTTTTTTTTTTTTTTTTWTTTTT TTp- m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02016.D HP022102.M Wed Feb 27 08:34:33 2002 Page 13

NYC-WTC_000004541

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NYC-WTC_000004541Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999