GCMS analysis results for sample AE03075, March 5 2002

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Library Search Compound Report * Data File : C:\MSDCHEM\1\5973N\02FEB28\02717.D Vial: 2 Acq On : 28 Feb 2002 3:30 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 N-perdeuteriobenzylideneani... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.10 ug/L 62034 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeut eriobenzy1ideneaniline 192 C13D11N 000538-51-2 64 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 50 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 8-(3-Hydroxyethyl)-3-methoxybicy... 192 C12H16O2 000000-00-0 47 Abundance Scan 1675 (22.283 min): 02717.D (-) m/z 192.10 100.00% 1512

5000

96 82 146 160 22.00 22.20 22.40 22.60 0 o— 4 n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 • >■।*»••।■ n * • • ■ । •1 • । mte ■ > 11111111111 m/z 191.00 17.98% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 110 m/z 96.00 17.86% 30 160 0 TT ■ ■ i" " i ■ ■ mP 1 94 ■" i1 “ • i ■ ‘ • • i ■ ■ ■' i"111'11111" " 1"1,11 Tgr n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102010:2,4-Diamino-6-(hydroxymethyI)pteridine

163 192 ..n. . 22.00 '22.20 22.40 22.60 5000 m/z 193.10 14.95% A 66 146 175 121 12= « 34 0 ‘ “ 1 ■1'11 •1 ■ ■ i ■ • ■ • i ■ ■ ’1’01210111000111—000000310000307 1. 135 All 11" iz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospho!in... 159 1512 22.00 22.20 22.40 22.60 m/z 146.10 13.20% 5000

144 177

miz—> 0 I'11" 11' , „ — .............................................. " ■i''" i ‘' i ■"' i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ‘ ■ i “ " i ■ ■ ■' i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■■ i ■ ■ i ■ ■ ■ ■ i■ "I1"' . Am . 22.00 22.20 22.40 22.60

02717.D HP022102.M Fri Mar 01 10:07:22 2002 Page 13

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