GCMS surrogate recovery results for sample AE03184, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report , Data File C:\MSDCHEM\l\5973N\02MAR01\03184.D Vial: 4 Acq On 1 Mar 2002 12:48 pm Operator: Sample 508 scan Inst : Ins t rumen Mise March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ************************ * ** * *** * * * ** ** *** **************************** Peak Number 9 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.13 ug/L 1462430 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87- 3 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 223 (5.891 min): 03184.D (-) m/ z 73.10 100.00% 7)3

5000 43 ' 1 ' i ' 1 ' ' i 1 ' 1 ' /dd 1 r1 । । । 5.60 5.80 6.00 6.20 ...................... 1 , 87 103 0- 11111 " 11111111111’f 111" 1 ’ 111111f TTOTTTTITTTT m/z 43.10 24.26% m/z-> 10 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 CTunmRRTmgm 5.60 5.80 6.00 6.20 43 m/z 41.10 9.22% 27 55

' _ V. 01" i1 "11 ■ " 1111" i'111 11" " i " ' , i ,1" i ■1187■ i H '111111 113 174 r'1111 ■ ■1111'1111 ■111 ■ Evt < • 111111111 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.19%

..1 43 2755 174 TTT 11" " i " ■11 ‘ , 01" i111 ■ i1 i' 87 113 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.50%

m/z-> 5000

0 15 r' 11 Hr 11' 44 58

TOTT—mmu]uuu 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 1 5.80 6.00 6.20

'3184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 11

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