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GCMS surrogate recovery results for sample AE03184, March 2002

Machine-extracted title · confidence 100%

Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.

NYC-WTC_000006045–000006064

Folder label: “GCMS X 2/12/02 A 3/01/02

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NYC 9/11 Public Portal Document 2 P—

Data File : C:\MSDCHEM\l\5973N\02MAR01\03184.D Vial: 4 Acq On : 1 Mar 2002 12:48 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.92 ug/L 472050 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 47 3 N-(Trifluoroacetyl)-N,O,0',0''-t... 553 C22H42F3NO4Si4 000000-00-0 47 4 N-(Trifluoroacetyl)-O,O',O''-tri... 481 C19H34F3NO4Si3 000000-00-0 38 Abundance Scan 812 (12.541 min): 03184.D (-) m/z 73.00 100.00% 73

5000 267 355 .............. .. ........................ ...........

45 | 12.20 12.40 12.60 12.80 109 154 193 223 , 323 i m/z 266.90 47.38% 0- ■ 'I ' ■ --r 11*21 Hi* fi m/z-> Abundance 50 73 100 150 200 250 300 350 400 450 #313068: Cyclopentasiloxane, decamethyl- 500 550 1 355 5000 267 .......... M.......... 12.20 12.40 12.60 12.80 m/z 355.00 45.87% 207 ...................................................... .. .................... ....... 0- ■ ■ i ' ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 ....... )....... | 12.20 12.40 12.60 12.80 5000 355 m/z 356.00 14.87% 44 147 193 267294 0- ' 1'1 1—————kn——B——a—B—B/BBdE—BBBDmn——TCCTTTTTGTT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #377151: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethyl... ......... 73 12.20 12.40 12.60 12.80 m/z 267.90 12.55% 355 5000

45 0 — —— „ ——————————————— 147 193 267 _ 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 12.20 12.40 12.60 12.80

03184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 12

NYC-WTC_000006060

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NYC-WTC_000006060Source: NYC Law Department, mirrored locally

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