GCMS analysis results for sample AE00168, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN24\00168.D Vial: 1 Acq Ori : 24 Jan 2002 2:59 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 Butenol, methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.01 0.11 ug/L 45260 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW Mol Form ‘ CAS# Qual l Butenol, methyl- 86 C5H10O 060766-00-9 72 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 56 3 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 50 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 9 Abundance Scan 143 (5.006 min): 00168. D (-) m/z 71.10 100.00% 43 71

5000 39 49 55 59 1 A. 1 ‘ I ‘ r‘ ‘ I ' 1 4.60 4.80 i ■ ■ > > i ‘ 5.00 5.20 ■ l 1 ■ 5.40 84 TI09000011—0—B——B31"T TH I “ 1 ‘ I “ T ' ■ ■ i • ■ ■ • i • ■ ‘11 ■1 *' I" ‘ ■ i m/z 43.10 98.35% /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- 43 71

5000 59 27 4.60 4.80 5.00 5.20 5.40 15 31 m/z 41.10 68.76% 53

m/z-> Abundance

5000 5 “ ' l‘ 1 "I' 1 11 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #4083:3-Buten-2-ol, 2-methyl-

27 31 1 “I 1 ‘ ‘ t' ‘

43 67. , -HHH TTH

59 71 86 1 ■' i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■11 ■' • ■ i

M 4.60 m/z 4.80 59.10 - 5.00 5.20 5.40 42.84%

n/z-> 5 ‘ ■ i ‘‘ ■ i ■ '' ■ ■ i'1' ‘ i ‘ -37+ 8 mpH "11010070111111211111111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4081:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... .A . A 7h 4.60 4.80 5.00 5.20 5.40 m/z 69.00 37.30% 43 5000 59 27 31 53 67 TTT-rp-rT-TTTTTTp-n-rjT TIPT7 TIWTTTTTTTT M • * 11 > IH ( ............ ................... m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

30168.D SCAN508.M Fri Jan 25 10:25:53 2002 Page 8

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