DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02385.D Vial: 1 Acq On : 27 Feb 2002 3:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 5-Fluoronicotin amide Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.07 ug/L 43901 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Fluoronicotin amide 140 C6H5FN20 000000-00-0 50 2 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-9 39 3 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 9 4 3H-Pyrazol-3-one, 2,4-dihydro-2,... 140 C7H12N20 003201-25-0 9 Abundance Scan 886 (13.376 min): 02385.D (-) m/z 140.00 100.00% 140

5000

‘ 11111 1 ‘‘ 11 ■ ■ i ■ 70 94 108 13.00 13.20 13.40 13.60 13.80 O+ 49 I.I 84 | T 1 ■ i ' ■ ■ ■ i ‘ ' 1 1 i ■ ‘ 1 1 I ' 1 1 ' i ' 1 ' 1 i 1 ' ' 1 I ■ ' ' 1 i ' 1 1 ' i ' 1 1 1 i 1 ‘ +L "tI m/z 70.00 12.24% m/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35137: 5-Fluoronicotin amide 140

96 5000 124 ..... i ' i ■ ' 1 1 i ■ ■ ■ > i ■ ■ • ■ i ■ 13.00 13.20 13.40 13.60 13.80 44 69 76 m/ z 94.10 12.04% — 50 A Of ■ ■ i 1 1111 ‘ 1* I ................... —L 1tT m/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35063: 2-Hydroxy-5-nitropyridine $$ 5-N'rtro-2-hydroxypyri... 140 m 13.00 13.20 13.40 13.60 13.80 5000 m/z 141.00 12.02% 66

80 93 110

mfe-> 01 ............ ............., ■ 1 । 1 1 ' 1 i ‘ 40 50 । 1 1 60 70 mb 80 90 1 1 1 i'1 1 1 1 1 100 110 120 130 ■ | I ■ ■ ' । 124 'I ■ ■ i 1 ■ —L "II 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 13.00 13.20 13.40 13.60 13.80 m/ z 66.00 8.78%

5000

44 71 123 86 96 112 0 । | ' 1 i 1 1 ■ i ■ ■11/1/1/1/*1//*///[/11//1/1/*/1/’/1/d/T 13T m/z-> 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

02385.D HP022102.M Thu Feb 28 08:47:03 2002 Page 13

NYC-WTC_000005022

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NYC-WTC_000005022Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999