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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/25/02
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GCMS analysis results for sample AE00105, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.

NYC-WTC_000050793–000050812

Folder label: “GCMS X 1/4/02 A 1/25/02”

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Scanned page image, NYC-WTC_000050809
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library searen compound Keport

Data File : C : \MSDCHEM\1\5973N\02JAN25\00105 . D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.05 ug/L 32693 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 38 4 N-(Trifluoroacetyl)-N, 0,0',0''-t... 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 803 (12.542 min): 00105.D (-) m/z 73.10 100.00% 73 A 5000 267 355 ।________________ ■ । • ■ • • । • • ■ • । ■ 12.20 12.40 12.60 12.80 49 ' i" " i J "' r " ■ r " ' r'" r'" r ' r "' i mPPT I1 II>|I I > I | ...T| I I . | | m/z 355.10 47.49% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ • । • • > • । • I ' ' 1 ' I ' ' ' 1 1 1 12.20 12.40 12.60 12.80 m/z 267.00 46.71% 207 323 ' I" " i ■' i" ■ • i ■ • • • । i • ■■ ■ i ■ ■ ■' l > ■ • • i ■ •" i ■ ■ ■ • । ..... .. . in "i"" i" " i" " । •i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T"’ 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 12.40% 355 45

m/z-> 4 r "' r " ■ r "' r " ■ r " ■ i" r ■■ ■ i"' 'r ' ii 193 223 IT 40 60 80 100120140160180200220240260280300320340360380400420440 I 323 k

Abundance #357156: Noradrenaline tetraTMS

MP T I ' 1 1 ■ I ' ' ' ■ I 1 73 12.20 1240 12.60 12.80 m/z83.90 9.92%

5000 102 355 MW

45

■n/z-> 4 147 40 60 80 100120140160180200220240260280300320340360380400420440 442 "i"' 12.20 1240 12.60 12.80

00105.D SCAN508.M Mon Jan 28 09:49:48 2002 Page 13

NYC-WTC_000050809

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NYC-WTC_000050809Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

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