Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
NYC-WTC_000050793–000050812Folder label: “GCMS X 1/4/02 A 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library searen compound Keport
Data File : C : \MSDCHEM\1\5973N\02JAN25\00105 . D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
12.54 0.05 ug/L 32693 Naphthalene-d8 13.19
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 38 4 N-(Trifluoroacetyl)-N, 0,0',0''-t... 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 803 (12.542 min): 00105.D (-) m/z 73.10 100.00% 73 A 5000 267 355 ।________________ ■ । • ■ • • । • • ■ • । ■ 12.20 12.40 12.60 12.80 49 ' i" " i J "' r " ■ r " ' r'" r'" r ' r "' i mPPT I1 II>|I I > I | ...T| I I . | | m/z 355.10 47.49% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313068: Cyclopentasiloxane, decamethyl- 73
355 267 5000 ■ • । • • > • । • I ' ' 1 ' I ' ' ' 1 1 1 12.20 12.40 12.60 12.80 m/z 267.00 46.71% 207 323 ' I" " i ■' i" ■ • i ■ • • • । i • ■■ ■ i ■ ■ ■' l > ■ • • i ■ •" i ■ ■ ■ • । ..... .. . in "i"" i" " i" " । •i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T"’ 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 12.40% 355 45
m/z-> 4 r "' r " ■ r "' r " ■ r " ■ i" r ■■ ■ i"' 'r ' ii 193 223 IT 40 60 80 100120140160180200220240260280300320340360380400420440 I 323 k
Abundance #357156: Noradrenaline tetraTMS
MP T I ' 1 1 ■ I ' ' ' ■ I 1 73 12.20 1240 12.60 12.80 m/z83.90 9.92%
5000 102 355 MW
45
■n/z-> 4 147 40 60 80 100120140160180200220240260280300320340360380400420440 442 "i"' 12.20 1240 12.60 12.80
00105.D SCAN508.M Mon Jan 28 09:49:48 2002 Page 13
NYC-WTC_000050809
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NYC-WTC_000051364
Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051236
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050664
Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050702
Administrative record from DEP Box 28 documenting CCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050703
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 4 and 25, 2002.
Filed in the same folder
NYC-WTC_000050705
Laboratory report listing concentrations of volatile organic compounds in sample AE00027 analyzed on January 25, 2002.
Filed in the same folder
NYC-WTC_000050709
Reference standard GCMS analysis for sample AE00027 performed on January 25, 2002, providing quality control results.
Filed in the same folder
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
Filed in the same folder